Microwave-assisted synthesis of hybrid organo-layered double hydroxides containing cholate and deoxycholate

2019 ◽  
Vol 225 ◽  
pp. 28-33 ◽  
Author(s):  
Daniel Cosano ◽  
Dolores Esquivel ◽  
Francisco J. Romero ◽  
César Jiménez-Sanchidrián ◽  
José Rafael Ruiz
2020 ◽  
Vol 179 ◽  
pp. 332-339
Author(s):  
Xiaohong Wang ◽  
Youzhi Tu ◽  
Liping Zhu ◽  
Lin Wu ◽  
Laxia Wu ◽  
...  

2012 ◽  
Vol 554-556 ◽  
pp. 532-535
Author(s):  
Chun Xia Chen ◽  
Kun Zhang ◽  
Bin Li

Cu-containing Layered Double Hydroxides (Cu-LDHs) prepared in a microwave field (Cu-LDHs-b) differs drastically according to the appearance, chemical component and the catalytic activity when compared with conventionally prepared sample (Cu-LDHs-a). From the TEM images, it is obvious that the particle size range of Cu-LDHs-b with 30~90 nm is narrower than that of Cu-LDHs-a with 30~120 nm, and the dispersibility of Cu-LDHs-b is better than that of Cu-LDHs-a. ICP-AES characterization shows that raw material utilization ratio of Cu-LDHs-b is higher than that of Cu-LDHs-a. Furthermore, Cu-LDHs-b exhibites higher catalytic activity than Cu-LDHs-a in the phenol hydroxylation with H2O2. Therefore, the microwave-assisted synthesis is an ideal method for synthesis of nano-Cu-LDHs.


2007 ◽  
Vol 180 (3) ◽  
pp. 873-884 ◽  
Author(s):  
M. Herrero ◽  
P. Benito ◽  
F.M. Labajos ◽  
V. Rives

2011 ◽  
Vol 239-242 ◽  
pp. 375-379 ◽  
Author(s):  
Chun Xia Chen ◽  
Yu Zhang ◽  
Han Qing Zhao ◽  
Jin Song Peng ◽  
Bin Li

Ce-containing Layered Double Hydroxides (Ce-LDHs) were prepared by conventional and microwave-assisted crystallization method, which were denoted as Ce-LDHs-A and Ce-LDHs-B, respectively. The dispersibility of Ce-LDHs-B is much better than that of Ce-LDHs-A; the particles of Ce-LDHs-B with particle size ranging from 20 to 70 nm are smaller than that of Ce-LDHs-A with sizes around 50-300 nm. The effect of the cerium to aluminum molar ratios, microwave crystallization time and reaction temperature on the structure of Ce-LDHs was also investigated. The results show the excessive Ce into LDHs causes distortion of the samdwich, the damage of the LDHs structure becomes more and more serious with increasing the proportion of Ce/Al. The structure of Ce-LDHs becomes more and more perfect with the increasing of the microwave crystallization time and reaction temperature.


RSC Advances ◽  
2016 ◽  
Vol 6 (41) ◽  
pp. 34534-34545 ◽  
Author(s):  
Ufana Riaz ◽  
S. M. Ashraf ◽  
Sanjay Kumar Saroj ◽  
Mohd Zeeshan ◽  
Sapana Jadoun

Intercalation of organic moieties in layered double hydroxides/clays has been used to obtain various hybrid compounds with enhanced properties and wide ranging applications.


2020 ◽  
Vol 5 (3) ◽  
pp. 506-518 ◽  
Author(s):  
Sonia Bujok ◽  
Magdalena Konefał ◽  
Sabina Abbrent ◽  
Ewa Pavlova ◽  
Jan Svoboda ◽  
...  

Layered double hydroxides with ionic liquid as highly active catalytic-initiating system for microwave-assisted ring opening polymerization of ε-caprolactone.


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