Role of grain boundary ferrite layer in dynamic recrystallization of semi-solid processed type 304L austenitic stainless steel

2016 ◽  
Vol 179 ◽  
pp. 65-68 ◽  
Author(s):  
Dipti Samantaray ◽  
Atanu Chaudhuri ◽  
Utpal Borah ◽  
A.K. Bhaduri ◽  
Pradip Dutta
Author(s):  
Ana I. Martinez-Ubeda ◽  
Ian Griffiths ◽  
Oliver D. Payton ◽  
Charles M. Younes ◽  
Tom B. Scott ◽  
...  

Intergranular creep cracks have been observed in the heat affected zone of the 316H austenitic stainless steel superheater boiler tube bifurcation weldments after long term service at temperature of ∼550°C. The cracking mechanism is believed to be creep dominated. Moreover, chemical composition of defective material compared with similar uncracked components suggests that composition influences susceptibility to creep cracking. A systematic characterization of ratios number of creep cavities/grain boundary length and inter-granular precipitation length/grain boundary length has been undertaken in HAZ of three samples extracted from plants with different specific compositions. Here, the role of precipitation on creep deformation and fracture is explored. Precipitates of both ferrite and M23C6 carbide arising from long term service and associated creep cavitation have been identified using transmission electron microscopy. The creep damage and cracking, and therefore overall service life creep, is discussed by consideration of susceptibility of creep cavity nucleation and subsequently growth arising from specific differences in the chemical composition of the three boiler tube bifurcations.


2009 ◽  
Vol 51 (9) ◽  
pp. 2144-2150 ◽  
Author(s):  
N. Parvathavarthini ◽  
S. Mulki ◽  
R.K. Dayal ◽  
I. Samajdar ◽  
K.V. Mani ◽  
...  

2011 ◽  
Vol 702-703 ◽  
pp. 714-717 ◽  
Author(s):  
Sumantra Mandal ◽  
A.K. Bhaduri ◽  
V. Subramanya Sarma

The origin and role of S3 boundaries during dynamic recrystallization (DRX) and grain boundary engineering (GBE) of a Ti-modified austenitic stainless steel (alloy D9) is studied. Hot deformation tests were carried out on solution-annealed (SA) specimens to study the DRX behavior whereas a series of cold deformation and annealing were performed on SA specimens to realize GBE microstructure. A linear relationship between the area fraction of DRX and the number fraction of Σ3 boundaries was observed during hot deformation. This high fraction of Σ3 boundaries could account for the formation of coherent annealing twins by “growth accidents” during DRX. For certain combinations of cold deformation and annealing, a significant increase in S3 boundaries was observed. In contrast to hot deformation, majority of these new S3 boundaries during cold deformation and annealing were formed by geometrical interactions between the pre-existing Σ3 boundaries. The role of the S3 boundaries during DRX and on tailoring microstructure through grain boundary engineering approach is discussed.


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