Synthesis and characterization of a high-purity chiral 5,5'-disulfonato-BINAP ligand and its application in asymmetric hydrogenation of β-keto esters

2021 ◽  
Vol 507 ◽  
pp. 111562
Author(s):  
Xin Jin ◽  
Sen Huang ◽  
Fan Wang ◽  
Lin Zhu ◽  
Hongbing Song ◽  
...  
2021 ◽  
Vol 14 (1) ◽  
pp. 39-47
Author(s):  
M. Fatih Polat ◽  
Derya Aktaş Anı

In this study, a new series consisting of 12 heteroaryl chalcone derivatives of 1,3,5-trimethoxybenzene were synthesised. Chalcones were synthesised in high purity and efficiency, via condensation of mono, bis and tris 2,4,6-trimethoxy acetophenones with hetero-2-carbaldehyde derivatives based on Claisen Schdmit condensation. The reactions feature a good scope for the all products, mild reaction conditions and good yields. The synthesized compounds were characterized by using FT-IR, NMR and elemental analysis spectroscopic techniques.


2021 ◽  
Vol 1 (1) ◽  
pp. 119-123
Author(s):  
Lilian Celeste Alarcón Segovia

Gold nanoparticles (AuNPs) find a number of applications in many fields of electronics, catalysis, optics and biomedicine. This work reports a robust, fast and easy synthesis protocol, based on the Turkevich method to obtain AuNPs. Simple characterization techniques based on UV-Vis spectroscopy and transmission electronic microscopy are also reported. The resulting AuNPs presents properties at a nanometric scale, high purity and they may find potential uses in the treatment of cancer, antiviral and antibacterial agents and biosensors among others.


2014 ◽  
Vol 40 (6) ◽  
pp. 8117-8123 ◽  
Author(s):  
Kyung-In Kim ◽  
Sung-Churl Choi ◽  
Jin-Ho Kim ◽  
Woo-Seok Cho ◽  
Kwang-Taek Hwang ◽  
...  

RSC Advances ◽  
2015 ◽  
Vol 5 (32) ◽  
pp. 24930-24935 ◽  
Author(s):  
L. Giri ◽  
G. Mallick ◽  
A. C. Jackson ◽  
M. H. Griep ◽  
S. P. Karna

Schematic solvothermal synthesis of Bi2Te3 (a) producing Bi2Te3 hexagonal nanoplates (TEM) (b) which was converted into pellet (c). The electrical characterization (d) of the Bi2Te3 pellet surface showed significantly high current (more than 100 times) than through the pellet.


2009 ◽  
Vol 26 (1) ◽  
pp. 281-284 ◽  
Author(s):  
Seung-Joon Yoo ◽  
Dong-Heui Kwak ◽  
Se-Il Lee ◽  
Jae-Wook Lee ◽  
Un-Yeon Hwang ◽  
...  

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