The influence of slow cooling on Y211 size and content in single-grain YBCO bulk superconductor through the infiltration-growth process

2017 ◽  
Vol 534 ◽  
pp. 37-44 ◽  
Author(s):  
A Ouerghi ◽  
N. Moutalbi ◽  
J.G. Noudem ◽  
A. M'chirgui
2017 ◽  
Vol 891 ◽  
pp. 489-493 ◽  
Author(s):  
Liudmila Vojtkova ◽  
Pavel Diko

Single grain YBCO bulk superconductors were prepared from different starting precursors. In the first case, Y2Ba1Cu1O5 (Y211) powder as the solid phase and the liquid phase of mixture of YBa2Cu3O7-x+BaCuO2+CuO powders were used. In the second case the solid phase was prepared from the mixture of Y2O3+BaCuO2 instead of the conventionally used Y211. The microstructure of samples was studied by polarized light microscopy and scanning electron microscope (SEM). The influence of different staring compositions on the final size of Y211 particles is shown. Also the influence of BaCuO2 concentration in the Y2O3+x·BaCuO2 (x=0.2; 0.5; 0.8; 1; 1.2; 1.5; 1.8) mixture on the Y211 size was studied.


2010 ◽  
Vol 470 (2) ◽  
pp. 155-158 ◽  
Author(s):  
P. Diko ◽  
V. Antal ◽  
M. Kaňuchová ◽  
M. Jirsa ◽  
K. Jurek

Author(s):  
Guo-Zheng Li ◽  
Miao Wang

Abstract A novel preform compaction method based on one new type of divisible mould was employed for fabricating single-grain YBCO bulk superconductor, which can complete the preform demoulding process through opening of the mould, rather than pushing the preform out in the regular mould. Thus it has natural superiority on eliminating macro-cracks, which has been proved by the sample surface morphology and the trapped field characterization. In addition, the divisible mould pressed sample exhibits higher levitation force and trapped field properties than the regular mould pressed samples, verifying the potentials of the divisible mould on improving the bulk performance. The optical micrograph results prove the superiority of the divisible mould on eliminating tiny cracks on sample surface. The processing facility and sample reliability brought by the divisible mould should also be emphasized, because the crushing and re-pressing of preform when it presents visible cracks can be omitted and the failed samples with surface cracks will no longer appear. Consequently, the experimental efficiency and stability are both enhanced.


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