Separating an overlapped 1H peak and identifying its 1H-1H correlations with the use of single-channel 1H solid-state NMR at fast MAS

2022 ◽  
pp. 101774
Author(s):  
Nghia Tuan Duong ◽  
Vipin Agarwal ◽  
Yusuke Nishiyama
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Single Channel ◽  
Fast Mas

Rapid Characterization of Formulated Pharmaceuticals Using Fast MAS 1H Solid-State NMR Spectroscopy

2019 ◽  
Vol 16 (7) ◽  
pp. 3121-3132 ◽  
Author(s):  
David A. Hirsh ◽  
Anuradha V. Wijesekara ◽  
Scott L. Carnahan ◽  
Ivan Hung ◽  
Joseph W. Lubach ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Solid State Nmr Spectroscopy ◽  
Fast Mas ◽  
Rapid Characterization

Slow and Very Fast MAS Solid State NMR Study of Biopolymers

2014 ◽  
Vol 339 (1) ◽  
pp. 60-69 ◽  
Author(s):  
Tomasz Pawlak ◽  
Piotr Paluch ◽  
Agata Jeziorna ◽  
Grzegorz D. Bujacz ◽  
Marek J. Potrzebowski
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Study ◽  
Fast Mas

scholarly journals Rapid acquisition of wideline MAS solid-state NMR spectra with fast MAS, proton detection, and dipolar HMQC pulse sequences

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Pulse Sequences ◽  
Quadrupolar Nuclei ◽  
Proton Detection ◽  
Rapid Acquisition ◽  
Half Integer ◽  
Fast Mas

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.

Structure determination of Ba5AlF13 by coupling electron, synchrotron and neutron powder diffraction, solid-state NMR and ab initio calculations

2016 ◽  
Vol 45 (39) ◽  
pp. 15565-15574 ◽  
Author(s):  
Charlotte Martineau ◽  
Mathieu Allix ◽  
Matthew R. Suchomel ◽  
Florence Porcher ◽  
François Vivet ◽  
...  
Keyword(s):  
Solid State ◽  
Dft Calculations ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
Neutron Powder Diffraction ◽  
Complementary Information ◽  
Electron Synchrotron ◽  
Structure And Dynamics ◽  
Fast Mas

The structure and dynamics of Ba5AlF13 are resolved by combining complementary information from powder diffraction, 27Al and 19F ultra-fast MAS NMR and DFT calculations.

Fast acquisition of multi-dimensional spectra in solid-state NMR enabled by ultra-fast MAS

2009 ◽  
Vol 196 (2) ◽  
pp. 133-141 ◽  
Author(s):  
Ségolène Laage ◽  
Joseph R. Sachleben ◽  
Stefan Steuernagel ◽  
Roberta Pierattelli ◽  
Guido Pintacuda ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Fast Acquisition ◽  
Fast Mas

Identifying H–N proximities in solid-state NMR using 14N overtone irradiation under fast MAS

CrystEngComm ◽  
2013 ◽  
Vol 15 (43) ◽  
pp. 8657 ◽  
Author(s):  
Luke A. O'Dell ◽  
Rongliang He ◽  
Jessica Pandohee
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Fast Mas
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