The detection and characterization of surface immobilized phosphine ligands and transition metal catalysts by high resolution 31P solid state NMR using magic angle spinning techniques

1982 ◽  
Vol 224 (1) ◽  
pp. C5-C9 ◽  
Author(s):  
L. Bemi ◽  
H.C. Clark ◽  
J.A. Davies ◽  
D. Drexler ◽  
C.A. Fyfe ◽  
...  
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Transition Metal ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Transition Metal Catalysts ◽  
Phosphine Ligands ◽  
Magic Angle ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

Characterization of Polymer Compatibility by1H Dipolar Filter Solid-State NMR under Fast Magic Angle Spinning

2007 ◽  
Vol 40 (25) ◽  
pp. 9018-9025 ◽  
Author(s):  
Xiaoliang Wang ◽  
Qiang Gu ◽  
Qing Sun ◽  
Dongshan Zhou ◽  
Pingchuan Sun ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Polymer Compatibility ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning
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