Reduction of carbonyl groups in aromatic polyketones: synthesis and characterization of methylene-bridged polyaryl-ethers and -thioethers

Polymer ◽  
1999 ◽  
Vol 40 (18) ◽  
pp. 5173-5182 ◽  
Author(s):  
Abderazzak Ben-Haida ◽  
Howard M. Colquhoun ◽  
Philip Hodge ◽  
David F. Lewis
2010 ◽  
Vol 2010 ◽  
pp. 1-7 ◽  
Author(s):  
K. C. Prousis ◽  
G. Athanasellis ◽  
V. Stefanou ◽  
D. Matiadis ◽  
E. Kokalari ◽  
...  

The synthesis and characterization of two new tetronic acid zinc (II) complexes of the empirical formulae [Zn(L–H)2(H2O)2] (1) and [Zn(L–H)2(H2O)(MeOH)]H2O(2) found within the same crystal are reported. The zinc ions bind through alkoxide and carbonyl groups of the ligand 3-methoxycarbonyl-5-phenyl tetronic acid (LH) as indicated byHNMR and X-ray crystallographic studies. These complexes promote intra- and intermolecular interactions, such as hydrogen bonding andπstacking, giving place to the formation of molecular aggregates.


1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.


2009 ◽  
Author(s):  
Marziye Javaheri Kachousangi ◽  
Rahmatollah Rahimi ◽  
Mohamad Mehdi Kashani-Motlagh

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