Spectroscopic characterization, electrochemistry and single-crystal structure of bis[chlorobis (dimethylphosphito-p)(hexamethylbenzene) ruthenium(II)-μ-(O,O,Cl)]Copper(II) dichloromethane (1:2), an unusual linear, heterotrinuclear complex

Polyhedron ◽  
1991 ◽  
Vol 10 (10) ◽  
pp. 1091-1096 ◽  
Author(s):  
Gerard A. Van Albada ◽  
Rudolf A.G. De Graaf ◽  
Ronald Hage ◽  
Jan Reedijk ◽  
Elke Buchholz ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Spectroscopic Characterization ◽  
Single Crystal Structure ◽  
Heterotrinuclear Complex

Single-crystal Structure Determination and Spectroscopic Characterization of KSr4(BO3)3

2013 ◽  
Vol 68 (4) ◽  
pp. 338-344 ◽  
Author(s):  
Gerhard Sohr ◽  
Doris Clara ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Single Crystals ◽  
Structure Determination ◽  
Normal Pressure ◽  
Spectroscopic Characterization ◽  
Single Crystal Structure ◽  
Crystal Structure Determination ◽  
Raman Spectroscopic ◽  
Pressure Phase

During attempts to synthesize a high-pressure phase of KSr4(BO3)3 using pressures of up to 12 GPa, single crystals of the normal-pressure phase KSr4(BO3)3 with sufficient quality for singlecrystal diffraction experiments could be obtained at 3 GPa and 1300 °C in a Walker-type multianvil apparatus. The single-crystal structure determination verified the published powder diffraction data of KSr4(BO3)3 revealing the non-centrosymmetric space group Ama2 with a = 1104:8(2), b=1199:1(2), c=688:8(2) pm and Z =4. Additionally, IR- and Raman-spectroscopic investigations were performed on single crystals of the compound.

Iron in kornerupine; a57Fe Moessbauer spectroscopic study and comparison with single-crystal structure refinement

1999 ◽  
Vol 84 (4) ◽  
pp. 536-549 ◽  
Author(s):  
Edward S. Grew ◽  
Guenther J. Redhammer ◽  
Georg Amthauer ◽  
Mark A. Cooper ◽  
Frank C. Hawthorne ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Spectroscopic Study ◽  
Structure Refinement ◽  
Single Crystal Structure ◽  
Crystal Structure Refinement

High‐pressure single‐crystal structure determinations for ruby up to 90 kbar using an automatic diffractometer

1978 ◽  
Vol 49 (8) ◽  
pp. 4411-4416 ◽  
Author(s):  
H. d’Amour ◽  
D. Schiferl ◽  
W. Denner ◽  
Heinz Schulz ◽  
W. B. Holzapfel
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Single Crystal ◽  
Single Crystal Structure ◽  
Structure Determinations ◽  
Automatic Diffractometer

Crystal and powder XRD data of Mg3(PO4)2-III: High-temperature and high-pressure form

1995 ◽  
Vol 10 (4) ◽  
pp. 293-295 ◽  
Author(s):  
F. Brunet ◽  
C. Chopin ◽  
A. Elfakir ◽  
M. Quarton
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Single Crystal ◽  
Diffraction Pattern ◽  
Structure Refinement ◽  
Powder Xrd ◽  
Single Crystal Structure ◽  
Crystal Structure Refinement ◽  
Pressure Form

A new diffraction pattern of the high-temperature and high-pressure polymorph Mg3(PO4)2-III (PDF 43-500) is given and indexed on the basis of a single-crystal structure refinement. It allows diffractogram indexing of the isostructural high-temperature and high-pressure form of Co3(PO4)2 (PDF 43-499).

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