Exploiting the Versatility of Ionic Liquids in Separation Science: Determination of Low-Volatility Aliphatic Hydrocarbons and Fatty Acid Methyl Esters Using Headspace Solid-Phase Microextraction Coupled to Gas Chromatography

2009 ◽  
Vol 81 (16) ◽  
pp. 7107-7112 ◽  
Author(s):  
Yunjing Meng ◽  
Verónica Pino ◽  
Jared L. Anderson
Keyword(s):  
Gas Chromatography ◽  
Ionic Liquids ◽  
Fatty Acid ◽  
Solid Phase Microextraction ◽  
Fatty Acid Methyl Esters ◽  
Solid Phase ◽  
Methyl Esters ◽  
Separation Science ◽  
Acid Methyl

On the determination of the distillation curve of fatty acid methyl esters by gas chromatography

Fuel ◽  
2022 ◽  
Vol 314 ◽  
pp. 123143
Author(s):  
Rodica Niculescu ◽  
Mihaela Năstase ◽  
Adrian Clenci
Keyword(s):  
Gas Chromatography ◽  
Fatty Acid ◽  
Fatty Acid Methyl Esters ◽  
Methyl Esters ◽  
Distillation Curve ◽  
Acid Methyl

Direct ultrasound-assisted methylation of fatty acids in serum for free fatty acid determinations

2010 ◽  
Vol 88 (9) ◽  
pp. 898-905 ◽  
Author(s):  
Liyan Liu ◽  
Ying Li ◽  
Rennan Feng ◽  
Changhao Sun
Keyword(s):  
Mass Spectrometry ◽  
Fatty Acids ◽  
Gas Chromatography ◽  
Fatty Acid ◽  
Fatty Acid Methyl Esters ◽  
Methyl Esters ◽  
Ultrasonic Waves ◽  
Acid Methyl ◽  
Ultrasound Assisted

A method for simultaneous determination of 16 free fatty acids (FFAs) in serum is described. The method involves conversion of FFAs to fatty acid methyl esters (FAMEs) using the heat of ultrasonic waves followed by gas chromatography and mass spectrometry (GC–MS) analysis. Optimum levels of the variables affecting the yield of FAMEs were investigated. The results indicate that the optimal levels are 55 °C, 60 W, 10% H2SO4/CH3OH, and 50 min. Recoveries ranged from 85.32% to 112.11%, with a detection limit ranging from 0.03 to 0.08 μg mL–1. The linearity, using the linear correlation coefficient, was higher than 0.9914.

Ionic liquids as stationary phases for fatty acid analysis by gas chromatography

The Analyst ◽  
2017 ◽  
Vol 142 (24) ◽  
pp. 4601-4612 ◽  
Author(s):  
C. Fanali ◽  
G. Micalizzi ◽  
P. Dugo ◽  
L. Mondello
Keyword(s):  
Gas Chromatography ◽  
Ionic Liquid ◽  
Ionic Liquids ◽  
Fatty Acid ◽  
Fatty Acid Methyl Esters ◽  
Stationary Phases ◽  
Methyl Esters ◽  
Fatty Acid Analysis ◽  
Gc Analysis ◽  
Acid Methyl

The present paper provides an overview of the application of ionic liquid (IL) columns for GC analysis of fatty acid methyl esters (FAMEs).

Sign in / Sign up

Export Citation Format

Share Document