Stopped flow Fourier transform nuclear magnetic resonance spectroscopy. Application to the .alpha.-chymotrypsin-catalyzed hydrolysis of tert-butyl-L-phenylalanine

1975 ◽  
Vol 97 (2) ◽  
pp. 273-276 ◽  
Author(s):  
John J. Grimaldi ◽  
Brian D. Sykes

1996 ◽  
Vol 79 (2) ◽  
pp. 423-425 ◽  
Author(s):  
George A Moniz ◽  
Gerald B Hammond

Abstract A new method for the separation and identification of ambrein in ambergris using adsorption chromatography and 1H and 13C Fourier transform nuclear magnetic resonance spectroscopy (FT-NMR) is presented. We demonstrated the effectiveness of this method by analyzing an approximately 85-year-old sample of suspected ambergris from the New Bedford Whaling Museum (New Bedford, MA). Results prove that ambrein remains a major constituent of ambergris even after 85 years of storage under ordinary conditions.



1978 ◽  
Vol 17 (4) ◽  
pp. 980-987 ◽  
Author(s):  
Gary J. Schrobilgen ◽  
John H. Holloway ◽  
Pierre Granger ◽  
Christian Brevard




Sign in / Sign up

Export Citation Format

Share Document