Determination of Multiple Torsion-Angle Constraints in U−13C,15N-Labeled Peptides:  3D1H−15N−13C−1H Dipolar Chemical Shift NMR Spectroscopy in Rotating Solids

2002 ◽  
Vol 124 (40) ◽  
pp. 11908-11922 ◽  
Author(s):  
Chad M. Rienstra ◽  
Morten Hohwy ◽  
Leonard J. Mueller ◽  
Christopher P. Jaroniec ◽  
Bernd Reif ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Torsion Angle

scholarly journals Determination of 15N Chemical Shift Anisotropy from a Membrane-Bound Protein by NMR Spectroscopy

2012 ◽  
Vol 116 (24) ◽  
pp. 7181-7189 ◽  
Author(s):  
Manoj Kumar Pandey ◽  
Subramanian Vivekanandan ◽  
Shivani Ahuja ◽  
Kumar Pichumani ◽  
Sang-Choul Im ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Chemical Shift Anisotropy ◽  
Membrane Bound

Quantitative Γ-HCNCH: determination of the glycosidic torsion angle χ in RNA oligonucleotides from the analysis of CH dipolar cross-correlated relaxation by solution NMR spectroscopy

2007 ◽  
Vol 39 (1) ◽  
pp. 17-29 ◽  
Author(s):  
Jörg Rinnenthal ◽  
Christian Richter ◽  
Jan Ferner ◽  
Elke Duchardt ◽  
Harald Schwalbe
Keyword(s):  
Nmr Spectroscopy ◽  
Torsion Angle ◽  
Solution Nmr ◽  
Solution Nmr Spectroscopy ◽  
Glycosidic Torsion Angle

scholarly journals Determination of relative tensor orientations by γ-encoded chemical shift anisotropy/heteronuclear dipolar coupling 3D NMR spectroscopy in biological solids

2010 ◽  
Vol 12 (45) ◽  
pp. 14873 ◽  
Author(s):  
Guangjin Hou ◽  
Sivakumar Paramasivam ◽  
In-Ja L. Byeon ◽  
Angela M. Gronenborn ◽  
Tatyana Polenova
Keyword(s):  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Dipolar Coupling ◽  
Chemical Shift Anisotropy ◽  
3D Nmr ◽  
Biological Solids

Chemical Shift Nonequivalence of Enantiomers of Amino Acid Derivatives in 1H NMR and 19F NMR Spectroscopy Induced by L-Chirasil- Val.

1992 ◽  
Vol 47 (7) ◽  
pp. 1034-1036 ◽  
Author(s):  
Bernhard Koppenhoefer ◽  
Michael Hummel
Keyword(s):  
Amino Acid ◽  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Methyl Esters ◽  
Enantiomeric Purity ◽  
Peak Splitting ◽  
H Nmr ◽  
Acid Methyl ◽  
Amino Acid Methyl Esters

Enantiomers of N-trifluoroacetyl-amino acid methyl esters in CC14 solution, after addition of the chiral polysiloxane (L)-Chirasil-Val, display a chemical shift nonequivalence ΔΔδ in both 1H NMR and 19F NMR spectroscopy. The effects found for the leucine and valine derivatives can be correlated with the thermodynamic parameters of interaction in the undiluted system, as determined by gas chromatography. In CDC13 solution, no peak splitting was observed. The method is potentially useful for the determination of the enantiomeric purity of substrates of low volatility.

Determination of nitrogen chemical shift anisotropy from the second-order cross-term in 14N MAS NMR spectroscopy

2003 ◽  
Vol 377 (3-4) ◽  
pp. 426-432 ◽  
Author(s):  
Tania Giavani ◽  
Henrik Bildsøe ◽  
Jørgen Skibsted ◽  
Hans J. Jakobsen
Keyword(s):  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Chemical Shift Anisotropy ◽  
Second Order ◽  
Mas Nmr ◽  
Cross Term

Determination of the Peptide Torsion Angle φ by15N Chemical Shift and13Cα-1HαDipolar Tensor Correlation in Solid-State MAS NMR

1998 ◽  
Vol 135 (1) ◽  
pp. 169-177 ◽  
Author(s):  
M. Hong ◽  
J.D. Gross ◽  
W. Hu ◽  
R.G. Griffin
Keyword(s):  
Solid State ◽  
Chemical Shift ◽  
Torsion Angle ◽  
Mas Nmr ◽  
Tensor Correlation
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