Synthesis, Crystal Structure, Thermal Decomposition, and 11B MAS NMR Characterization of Mg(BH4)2(NH3BH3)2

2014 ◽  
Vol 118 (23) ◽  
pp. 12141-12153 ◽  
Author(s):  
Lars H. Jepsen ◽  
Voraksmy Ban ◽  
Kasper T. Møller ◽  
Young-Su Lee ◽  
Young Whan Cho ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Mas Nmr ◽  
Nmr Characterization

Crystal Structure, Infrared and Solid State CP MAS NMR Characterization of [(PPh3)2AgO2CH] and of [(PPh3)2AgO2CH].cntdot.2HCO2H, a Complex of the H-Bonded [H2(HCO2)3]- Species

1995 ◽  
Vol 99 (12) ◽  
pp. 3909-3917 ◽  
Author(s):  
Graham A. Bowmaker ◽  
Effendy ◽  
John V. Hanna ◽  
Peter C. Healy ◽  
Graeme J. Millar ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Solid State ◽  
Mas Nmr ◽  
Nmr Characterization ◽  
Cp Mas Nmr

MAS NMR characterization of syndiotactic polypropylene: crystal structure and amorphous phase conformation

1993 ◽  
Vol 26 (21) ◽  
pp. 5782-5789 ◽  
Author(s):  
Piero Sozzani ◽  
Roberto Simonutti ◽  
Maurizio Galimberti
Keyword(s):  
Crystal Structure ◽  
Amorphous Phase ◽  
Mas Nmr ◽  
Syndiotactic Polypropylene ◽  
Nmr Characterization

scholarly journals 29Si and 27Al MAS NMR Characterization of the Structural Evolution of a Lateritic Clay under Acidic and Alkaline Treatments

2018 ◽  
Vol 07 (01) ◽  
Author(s):  
Herve Goure Doubi ◽  
Valerie Montouillout ◽  
Gisele L Lecomte Nana ◽  
Benoit Nait Ali ◽  
Leon Koffi Konan ◽  
...  
Keyword(s):  
Structural Evolution ◽  
Mas Nmr ◽  
Lateritic Clay ◽  
27Al Mas Nmr ◽  
Nmr Characterization

scholarly journals Einkristallzüchtung und Röntgenstrukturanalyse polymerer 1:1-Komplexe von CuBr2 und CuCl2 mit Pyrazin aus Gelen / Crystal Growth in Gels and X-Ray Characterization of Polymeric 1:1-Complexes of CuBr2 and CuCl2 with Pyrazine

1989 ◽  
Vol 44 (5) ◽  
pp. 553-556 ◽  
Author(s):  
Th. Fetzer ◽  
A. Lentz ◽  
T. Debaerdemaeker
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Crystal Growth ◽  
Chloro Complex ◽  
Monoclinic Space Group ◽  
Crystal Data ◽  
Space Group ◽  
X Ray ◽  
Linear Chains

Single crystals of Cu(pz)Br2 and Cu(pz)Cl2 were grown by using gel methods with tetramethoxysilane as the gel-forming reagent. Thermal decomposition is interpreted. Crystal data for the bromo complex: monoclinic, space group C2/m with a = 1239.2(3) pm, b = 685.9(2) pm, c = 390.7(3) pm, β = 96,23(5)°. Crystal data for the chloro-complex: monoclinic, space group C2/m with a = 1197.1(3) pm, b = 684.9(3) pm, c = 370.1(3) pm, β = 95.96(5)°. Crystal structure analyses reveal that CuHal2 molecules are bonded by pyrazine to form linear chains. These chains are cross-linked by bridging halogen atoms.

Synthesis, crystal structure, and advanced NMR characterization of a low temperature polymorph of SiSe2

2016 ◽  
Vol 4 (29) ◽  
pp. 11276-11283 ◽  
Author(s):  
Jian Wang ◽  
Maxwell Marple ◽  
Kathleen Lee ◽  
Sabyasachi Sen ◽  
Kirill Kovnir
Keyword(s):  
Crystal Structure ◽  
Low Temperature ◽  
Nmr Characterization

scholarly journals The accuracy challenge of the DFT-based molecular assignment of 13C MAS NMR characterization of surface intermediates in zeolite catalysis

2020 ◽  
Vol 22 (41) ◽  
pp. 24004-24013
Author(s):  
Alexander A. Kolganov ◽  
Anton A. Gabrienko ◽  
Ivan Yu. Chernyshov ◽  
Alexander G. Stepanov ◽  
Evgeny A. Pidko
Keyword(s):  
Mas Nmr ◽  
Method Choice ◽  
Zeolite Catalysis ◽  
13C Mas Nmr ◽  
Nmr Characterization ◽  
Surface Intermediates

The influence of model and method choice on the DFT-computed NMR signatures of intrazeolite methoxide intermediates was investigated.

Quantitative MAS NMR characterization of the LiMn1/2Ni1/2O2 electrode/electrolyte interphase

2012 ◽  
Vol 42 ◽  
pp. 51-61 ◽  
Author(s):  
M. Cuisinier ◽  
J.-F. Martin ◽  
P. Moreau ◽  
T. Epicier ◽  
R. Kanno ◽  
...  
Keyword(s):  
Mas Nmr ◽  
Nmr Characterization

Synthesis and Characterization of Co Nanoparticles by Solventless Thermal Decomposition

2007 ◽  
Vol 119 ◽  
pp. 71-74 ◽  
Author(s):  
Yan Li ◽  
Xiao Li Zhang ◽  
Young Hwan Kim ◽  
Young Soo Kang
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Synthesis And Characterization ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Structure Of Nanoparticles ◽  
Co Nanoparticles

Co nanoparticles were synthesized via a solventless thermal decomposition of Co2+-oleate2. The crystalline structure is strongly affected by the thermal treatment of the Co nanoparticles. Further, the annealing also results in the decomposition of surfactant around Co particles. The size of nanoparticles was confirmed by transmission electron microscopy (TEM). The crystal structure of nanoparticles was characterized by X-ray diffraction pattern (XRD). The magnetic properties were characterized by vibrating sample magnetometer (VSM).

scholarly journals Einkristallzüchtung und Röntgenstrukturanalyse des polymeren 1:1-Komplexes zwischen CuCl2 und Pyridazin / Crystal Growth in Gels and X-Ray Characterization of the Polymeric 1:1-Complex of CuCl2 with Pyridazine

1990 ◽  
Vol 45 (2) ◽  
pp. 199-202 ◽  
Author(s):  
Th. Fetzer ◽  
A. Lentz ◽  
T. Debaerdemaeker ◽  
O. Abou-El-Wafa
Keyword(s):  
Crystal Structure ◽  
Thermal Decomposition ◽  
Crystal Growth ◽  
Single Crystals ◽  
Crystal Structure Analysis ◽  
Van Der Waals Interactions ◽  
Monoclinic Space Group ◽  
Crystal Data ◽  
X Ray

Single crystals of Cu(pdz)Cl2 were grown by using gel methods with tetramethoxysilane as the gel-forming reagent. Thermal decomposition is interpreted. Crystal data for the complex : monoclinic, space group C2/c with a = 938.3(3) pm, b = 1242.9(3) pm, c = 675.7(4) pm, β = 128.48(5)°. A crystal structure analysis reveals CuCl2 molecules connected by pyridazine in the form of zigzag-chains. Between these chains there are only Van-der-Waals-Interactions.

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