Stereocomplex formation between enantiomeric poly(lactic acid)s. 7. Phase structure of the stereocomplex crystallized from a dilute acetonitrile solution as studied by high-resolution solid-state carbon-13 NMR spectroscopy

1992 ◽  
Vol 25 (16) ◽  
pp. 4114-4118 ◽  
Author(s):  
Hideto Tsuji ◽  
Fumitaka Horii ◽  
Masaru Nakagawa ◽  
Yoshito Ikada ◽  
Hisashi Odani ◽  
...  
Keyword(s):  
Lactic Acid ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Phase Structure ◽  
Acetonitrile Solution ◽  
Poly Lactic Acid ◽  
Stereocomplex Formation

Structural study of poly(vinyl alcohol) in the gel state by high-resolution solid-state 13C NMR spectroscopy

1995 ◽  
Vol 28 (19) ◽  
pp. 6677-6679 ◽  
Author(s):  
Masatoshi Kobayashi ◽  
Isao Ando ◽  
Takahiro Ishii ◽  
Shigetoshi Amiya
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Structural Study ◽  
13C Nmr ◽  
Vinyl Alcohol ◽  
13C Nmr Spectroscopy ◽  
Poly Vinyl Alcohol ◽  
Solid State 13C Nmr

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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