Hydrothermal synthesis of a rutile/anatase TiO2mixed crystal from potassium titanyl oxalate: crystal structure and formation mechanism

CrystEngComm ◽  
2018 ◽  
Vol 20 (24) ◽  
pp. 3363-3369 ◽  
Author(s):  
Kangkai Hu ◽  
Lei E ◽  
Dan Zhao ◽  
Chaoyang Hu ◽  
Jin Cui ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Formation Mechanism ◽  
Mixed Crystal ◽  
Titanyl Oxalate

Nowadays, rutile TiO2or anatase TiO2is prepared from titanium oxalate, but there are only few studies on the rutile/anatase TiO2mixed crystal.

ZnIO3(OH): a new layered noncentrosymmetric polar iodate – hydrothermal synthesis, crystal structure, and second-harmonic generating (SHG) properties

2012 ◽  
Vol 41 (27) ◽  
pp. 8348 ◽  
Author(s):  
Dong Woo Lee ◽  
Saet Byeol Kim ◽  
Kang Min Ok
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Second Harmonic

Hydrothermal Synthesis and X-ray Crystal Structure of Four Inorganic-Organic Hybrid Compounds in Vanadium /Copper Iodate Family

2008 ◽  
Vol 634 (9) ◽  
pp. 1601-1607
Author(s):  
Xiaomin Liu ◽  
Guanghua Li ◽  
Minghui Bi ◽  
Yawei Hu ◽  
Yang Yu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
X Ray ◽  
Organic Hybrid ◽  
Hybrid Compounds

The first proof of protonated anion tetrahedra in the tsumcorite-type compounds

2004 ◽  
Vol 68 (5) ◽  
pp. 757-767 ◽  
Author(s):  
T. Mihajlović ◽  
H. Effenberger
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Single Crystal ◽  
Diffraction Data ◽  
Title Compound ◽  
Monoclinic Space Group ◽  
X Ray Diffraction ◽  
Hydrogen Atoms ◽  
Synthetic Compounds ◽  
X Ray

AbstractHydrothermal synthesis produced the new compound SrCo2(AsO4)(AsO3OH)(OH)(H2O). The compound belongs to the tsumcorite group (natural and synthetic compounds with the general formula M(1)M(2)2(XO4)2(H2O,OH)2; M(1)1+,2+,3+ = Na, K, Rb, Ag, NH4, Ca, Pb, Bi, Tl; M(2)2+,3+ = Al, Mn3+, Fe3+, Co, Ni, Cu, Zn; and X5+,6+ = P, As, V, S, Se, Mo). It represents (1) the first Sr member, (2) the until now unknown [7]-coordination for the M(1) position, (3) the first proof of (partially) protonated arsenate groups in this group of compounds, and (4) a new structure variant.The crystal structure of the title compound was determined using single-crystal X-ray diffraction data. The compound is monoclinic, space group P21/a, with a = 9.139(2), b = 12.829(3), c = 7.522(2) Å, β = 114.33(3)°, V = 803.6(3) Å3, Z = 4 [wR2 = 0.065 for 3530 unique reflections]. The hydrogen atoms were located experimentally.

Hydrothermal synthesis, crystal structure and thermal transformation of a new zinc arsenate hydrate, Zn9(AsO4)6·4H2O †

1998 ◽  
pp. 527-532 ◽  
Author(s):  
Torben R. Jensen ◽  
Poul Norby ◽  
Jonathan C. Hanson ◽  
Eivind M. Skou ◽  
P. C. Stein
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Thermal Transformation

A Novel Layered Mixed-Valence Vanadium Phenanthroline Complex: Hydrothermal Synthesis and Crystal Structure of [VIVVV2O7(phen)]n

1995 ◽  
Vol 34 (1) ◽  
pp. 1-2 ◽  
Author(s):  
Chung-ying Duan ◽  
Yu-peng Tian ◽  
Zhong-lin Lu ◽  
Xiao-zeng You ◽  
Xiao-ying Huang
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Mixed Valence ◽  
Synthesis And Crystal Structure ◽  
Phenanthroline Complex

α-Fe2O3 nanoplates: PEG-600 assisted hydrothermal synthesis and formation mechanism

2011 ◽  
Vol 509 (3) ◽  
pp. 885-890 ◽  
Author(s):  
Guo-Ying Zhang ◽  
Yan-Yan Xu ◽  
Dong-Zhao Gao ◽  
Ya-Qiu Sun
Keyword(s):  
Hydrothermal Synthesis ◽  
Formation Mechanism ◽  
Peg 600

Hydrothermal synthesis and crystal structure of a hybrid material based on [Co4(phen)8(H2O)2(HPO3)2]4+ and a highly reduced polyoxoanion

2002 ◽  
pp. 2916-2920 ◽  
Author(s):  
Mei Yuan ◽  
Yangguang Li ◽  
Enbo Wang ◽  
Ying Lu ◽  
Changwen Hu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Hybrid Material ◽  
Synthesis And Crystal Structure
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