13C–13C spin-coupling constants in crystalline 13C-labeled saccharides: conformational effects interrogated by solid-state 13C NMR spectroscopy
Keyword(s):
C Nmr
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Solid-state 13C NMR reveals differences in O-glycosidic linkage conformation in solution and in crystalline disaccharides. Experimental JCC values in crystalline samples provide a means of validating JCC calculated from density functional theory.
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