Revealing hidden features of a Japanese articulated iron lobster via non-destructive local element analysis and 3D imaging

Author(s):  
László Szentmiklósi ◽  
Zoltán Kis ◽  
Manako Tanaka ◽  
Boglárka Maróti ◽  
Masato Hoshino ◽  
...  

We present a workflow to non-destructively determine the elemental compositions of internal volumes of interest enclosed within complex-shaped objects, by combining 3D X-ray or neutron imaging, prompt-gamma activation analysis, and...

2018 ◽  
Author(s):  
Zoltán Kis ◽  
Katalin Gméling ◽  
Tímea Kocsis ◽  
János Osán ◽  
Mihály András Pocsai ◽  
...  

We present precise analysis of major and trace elements of the humic acid. We used three different element analytical techniques in our investigations as prompt-gamma activation analysis (PGAA), neutron activation analysis (NAA) and X-ray fluorescence (XRF) analysis was carried out. We identified 42 elements in our sample.


Heritage ◽  
2019 ◽  
Vol 2 (1) ◽  
pp. 836-847 ◽  
Author(s):  
Daniela Di Martino ◽  
Enrico Perelli Cippo ◽  
Antonella Scherillo ◽  
Zsolt Kasztovszky ◽  
Ildikó Harsányi ◽  
...  

The production and manufacturing techniques of metals involve expertise, and the study of ancient artifacts relies on interdisciplinary skills. Metalworking processes used in the production of jewelry masterpieces can, for example, give indications on the provenance of an ancient object of an unknown origin and the techniques used. In this regard, metallic samples from the Chiaravalle Cross (a beautiful processional cross with a complex structure, dating to the 13th century) have been studied, combining bulk and point measurements. Neutron-based experiments (like Prompt Gamma Activation Analysis and neutron diffraction) provide the bulk of the elemental and mineralogical composition, while particle induced X-ray emission analyses evidenced important details on its manufacturing techniques.


2003 ◽  
Vol 18 (10) ◽  
pp. 2486-2493 ◽  
Author(s):  
H. Heather Chen-Mayer ◽  
William J. Heward ◽  
Rick L. Paul ◽  
Frederic J. Klug ◽  
Yan Gao

This paper describes two spatially resolved analytical techniques for chlorine distribution analysis in high-purity quartz glass. The first, prompt gamma activation analysis (PGAA), to which most of this paper is devoted, is emphasized because a new neutron focusing technique has made this study feasible. Despite the low concentration of chlorine, the neutron absorption cross section for Cl is about 200 times greater than for Si, making Cl in Si an ideal system for PGAA. The second technique described is micro-x-ray fluorescence using a laboratory-based spectrometer. The results from each technique and their ability to quantify low levels of chlorine (400–1800 μg Cl/g SiO2) are described.


2019 ◽  
Vol 3 (2) ◽  
pp. 54 ◽  
Author(s):  
Akira Otsuki ◽  
Pedro Pereira Gonçalves ◽  
Christian Stieghorst ◽  
Zsolt Révay

This work aimed to characterize the deportment/concentration and liberation/association of the metals and light elements within mechanically processed waste printed circuit boards (PCBs) that hold the complex and heterogeneous structure and distribution of different material components. Waste PCBs passed through a series of mechanical processing (i.e., comminution and sieving) for metal recovery and were then characterized without further destroying the particles in order to capture their heterogeneity. The characterizations were performed in a laboratory and large-scale neutron facility. The results obtained with a portable X-ray fluorescence spectroscopy and prompt gamma activation analysis were compared and confirmed the good agreement and complementarities in general. The advantages and disadvantages of the two different methods were identified and discussed in this paper, in relation to their application to the analysis of mechanically processed PCB particles.


2021 ◽  
Vol 72 (1) ◽  
pp. 21-25
Author(s):  
Boglárka Maróti ◽  
György Káli

AbstractEight ornaments and a dagger were analyzed using completely non-destructive techniques to determine their alloy compositions and to draw conclusions about the production technology. Prompt-gamma activation analysis and time-of-flight neutron diffraction proved that the studied objects are tin-bronzes. Difference was observed in the amounts of ore-related minor components (arsenic, silver, nickel) of the objects belonging to the two distinct archaeological sites. Based on the diffraction analysis of the microstructure, the objects are casts that were exposed to different degrees of manufacturing to reach their final forms.


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