Synthesis and Characterization of Alumina–Zirconia Nanopowders via an Oxalate Route

2008 ◽  
Vol 23 (8) ◽  
pp. 777-781 ◽  
Author(s):  
J. Chandradass ◽  
Hoy-Yul Park ◽  
M. Balasubramanian ◽  
Dong-sik Bae
Keyword(s):  
Synthesis And Characterization ◽  
Zirconia Nanopowders ◽  
Oxalate Route

scholarly journals Synthesis and Characterization of CuO, TiO2, and CuO-TiO2 Mixed Oxide by a Modified Oxalate Route

2017 ◽  
Vol 2017 ◽  
pp. 1-10 ◽  
Author(s):  
Ekane Peter Etape ◽  
Lambi John Ngolui ◽  
Josepha Foba-Tendo ◽  
Divine Mbom Yufanyi ◽  
Beckley Victorine Namondo
Keyword(s):  
Aqueous Solution ◽  
Copper Oxide ◽  
Titanium Oxide ◽  
Mixed Oxide ◽  
Fruit Juice ◽  
Synthesis And Characterization ◽  
Decomposition Products ◽  
Complete Decomposition ◽  
Oxalate Route

Copper oxide (CuO), titanium oxide (TiO2), and Cu-doped TiO2 nanoparticles have been synthesized by pyrolysis of their corresponding precursors initially prepared by precipitation in aqueous solution using A. carambola fruit juice as a natural source of the precipitating agent (oxalate). The precursors were synthesized and characterized by FTIR, TGA, and PXRD. The results revealed that the precursors obtained were CuC2O4, TiO2(OH−)2C2O4, copper-doped titanium hydroxyl oxalate, and copper titanium hydroxyl oxalate. Complete decomposition for the as-prepared precursors containing titanium ions occurs at 600°C while impurity free copper oxalate decomposed at 450°C. The as-prepared precursors were decomposed and calcined at 600°C for 4 hours and the calcination products were characterized by XRD, SEM, and EDX. The results revealed the decomposition products to correspond to CuO, TiO2, Cu0.131Ti0.869O2, and CuO/TiO2.

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

Synthesis and characterization of zeolite-encapsulated porphyrins

2009 ◽  
Author(s):  
Marziye Javaheri Kachousangi ◽  
Rahmatollah Rahimi ◽  
Mohamad Mehdi Kashani-Motlagh
Keyword(s):  
Synthesis And Characterization
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