Evolution of liquid-bond strength in powder injection moulding compact during thermal debinding: numerical simulation

2004 ◽  
Vol 12 (2) ◽  
pp. 311-323 ◽  
Author(s):  
Ying Shengjie ◽  
Y C Lam ◽  
J C Chai
2012 ◽  
Vol 506 ◽  
pp. 238-241 ◽  
Author(s):  
J. Surawatthana ◽  
Nutthita Chuankrerkkul ◽  
Wantanee Buggakupta

Porous alumina (Al2O3) ceramics were fabricated by powder injection moulding process. The feedstocks, composed of 44 50 vol% of Al2O3 powder, could be prepared using a composite binder, consisting of polyethylene glycol (PEG) and polyvinyl butyral (PVB). Debindings were carried out using a combination of water leaching of the PEG and thermal debinding of the PVB. It was observed that the removal of the PEG was fast at the initial stage and more than 90 wt% of the PEG could be removed within 4 hours. Sintering was performed in argon atmosphere at 1600 °C. The sintered specimens had apparent porosity in range of 26-32 %, depending on the feedstock compositions. The flexural strength values were in range of 90-140 MPa while the hardness values were in range of 5-9 GPa. It was found that both the strength and hardness of the specimens were increased with increasing powder loading.


2020 ◽  
pp. 1-9
Author(s):  
Raphaël Côté ◽  
Mohamed Azzouni ◽  
Oussema Ghanmi ◽  
Sarthak Kapoor ◽  
Vincent Demers

2011 ◽  
Vol 43 (1) ◽  
pp. 9-20 ◽  
Author(s):  
B.S. Zlatkov ◽  
M.V. Nikolic ◽  
V. Zeljkovic ◽  
N. Obradovic ◽  
V.B. Pavlovic ◽  
...  

The powder injection moulding (PIM) technology is lately becoming more and more significant due to complex design possibilities and good repeatability. This technology requires optimization of all steps starting with material and binder, injection, debinding and sintering parameters. Sintering is one of the key links in this technology. The powder injection moulding process is specific as during feedstock injection powder particles mixed into the binder do not come into mechanical contact. Shrinkage during sintering of PIM samples is high. In this work we have analyzed and modeled the sintering process of isotropic PIM samples of Sr-hexaferrite. The Master Sintering Curve (MSC) principle has been applied to analyze sintering of two types of PIM Sr-hexaferrite samples with completely removed binder and only the extraction step of the debinding procedure (thermal debinding proceeding simultaneously with sintering). Influence of the heating rate on resulting sample microstructures has also been analyzed. Influence of the sintering time and temperature was analyzed using three different phenomenological equations.


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