Flower-inducing effects of benzoic acid and some related compounds in Lemna paucicostata 151

ChemInform ◽  
2010 ◽  
Vol 23 (3) ◽  
pp. no-no
Author(s):  
R. FILLER ◽  
W. K. GNANDT ◽  
W. CHEN ◽  
S. LIN

2008 ◽  
Vol 91 (5) ◽  
pp. 1025-1036 ◽  
Author(s):  
Mohammed Shahid Ali ◽  
Syed Rafiuddin ◽  
Muhammad Imran Munir ◽  
Mohsin Ghori ◽  
Aamer Roshanali Khatri

Abstract A reversed-phase high-performance liquid chromatographic method was developed for the simultaneous determination of benzoyl peroxide and the related compounds benzoic acid (BA), methylparaben, benzaldehyde, propylparaben, and ethyl benzoate. The compounds are separated on a column containing octadecyl silane chemically bonded to porous silica particles. The mobile phase is acetonitrilebuffer (45 + 55, v/v). Solutions are injected into the chromatographic system under isocratic conditions at a constant flow rate of 1.5 mL/min with UV detection at 235 nm. Analysis of stability samples showed rapid accumulation of BA by thermal degradation. A rationale has been established for the acceptable limit of BA in the formulation, which already contains BA (0.2) as a preservative. The proposed method is efficient and determines the active compound and 5 related compounds in a run time of 20 min. The method was validated according to the guidelines of the International Conference on Harmonization and demonstrated good agreement with the validation requirements.


1986 ◽  
Vol 50 (8) ◽  
pp. 2053-2059 ◽  
Author(s):  
Shozo FUJIOKA ◽  
Akira SAKURAI ◽  
Naotsugu SUGIMOTO ◽  
Isomaro YAMAGUCHI ◽  
Noboru MUROFUSHI ◽  
...  

1983 ◽  
Vol 24 (2) ◽  
pp. 241-246 ◽  
Author(s):  
S. Fujioka ◽  
I. Yamaguchi ◽  
N. Murofushi ◽  
N. Takahashi ◽  
S. Kaihara ◽  
...  

1964 ◽  
Vol 117 (2) ◽  
pp. 488-492 ◽  
Author(s):  
E. F. Rogers ◽  
R. L. Clark ◽  
H. J. Becker ◽  
A. A. Pessolano ◽  
W. J. Leanza ◽  
...  

1981 ◽  
Vol 46 (7) ◽  
pp. 1607-1613 ◽  
Author(s):  
Jiří Jílek ◽  
Josef Pomykáček ◽  
Jiřina Metyšová ◽  
Miroslav Protiva

The reaction of 2,3-dichlorothiophenol with 2-iodobenzoic acid gave 2-(2,3-dichlorophenylthio)benzoic acid (V) which was transformed in four steps to the homological acid IX. Cyclization resulted in 6,7-dichlorodibenzo[b,f]thiepin-10(11H)-one (X) which was converted via the alcohol XI to the trichloro compound XII. Substitution reactions of XII with 1-methylpiperazine and 1-(2-hydroxyethyl)piperazine afforded the title compound I and its hydroxyethyl analogue II. Reaction of the ketone X with 1-methylpiperazine and titanium tetrachloride gave the enamine III. Compounds I-III exhibit mild central depressant and relatively strong cataleptic activity.


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