Characterization of Old Nuclear Waste Packages Coupling Photon Activation Analysis and Complementary Non-Destructive Techniques

2014 ◽  
Vol 61 (4) ◽  
pp. 2137-2143 ◽  
Author(s):  
Frederick Carrel ◽  
Bruno Charbonnier ◽  
Romain Coulon ◽  
Frederic Laine ◽  
Stephane Normand ◽  
...  
Proceedings ◽  
2018 ◽  
Vol 2 (10) ◽  
pp. 564
Author(s):  
Tyler C. Borgwardt

Paleontological samples are rare and non-renewable, which makes the study of their chemical or physical characteristics require non-destructive methods. Physical characteristics are routinely studied with non-destructive methods; however, chemical studies tend to require destructive methods unless samples are very small or only the surface compositions are of interest. One potential technique for non-destructive elemental analysis is photon activation analysis (PAA). PAA is a versatile, broad-spectrum, multi-element analysis tool with low sensitivities, capable of analyzing large samples without any alteration, preserving the physical characteristics. Recent work has applied PAA to fossils and their source matrices in an attempt to correlate provenance through trace element analysis. PAA was shown to be non-consumptive and able to identify 20+ elements in samples with sub-ppm sensitivities. From that work, several lessons were learned and the non-destructivity of the technique was better characterized. PAA doesn’t have one standardized methodology, as it varies depending on the sample type. As such, from the lessons learned from the previous research, a standard method of applying PAA non-destructively to paleontological samples has been developed and will be presented in the following paper.


Minerals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 617
Author(s):  
Ivana Krausová ◽  
Jiří Mizera ◽  
Zdeněk Řanda ◽  
David Chvátil ◽  
Pavel Krist

This paper introduces instrumental photon activation analysis (IPAA) utilizing short-lived products of photonuclear reactions, mainly (γ, n) and (γ, p), initiated by bremsstrahlung from the MT-25 microtron. A rapid nondestructive IPAA method for geochemical major element analysis is introduced as a tool for the basic geochemical characterization of rocks. Procedures were developed and parameters such as beam energy and irradiation-decay-counting times optimized with a representative set of geochemical reference materials, and an optimized scheme was applied in analysis of various geological samples. A complete analytical scheme combined with long-time irradiation IPAA and the possibility of utilization of photoexcitation reactions (γ, γ′) are briefly outlined.


2021 ◽  
Vol 72 (1) ◽  
pp. 21-25
Author(s):  
Boglárka Maróti ◽  
György Káli

AbstractEight ornaments and a dagger were analyzed using completely non-destructive techniques to determine their alloy compositions and to draw conclusions about the production technology. Prompt-gamma activation analysis and time-of-flight neutron diffraction proved that the studied objects are tin-bronzes. Difference was observed in the amounts of ore-related minor components (arsenic, silver, nickel) of the objects belonging to the two distinct archaeological sites. Based on the diffraction analysis of the microstructure, the objects are casts that were exposed to different degrees of manufacturing to reach their final forms.


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