Fabrication of Open-Cell, Microcellular Silicon Carbide Ceramics by Carbothermal Reduction

2005 ◽  
Vol 88 (10) ◽  
pp. 2949-2951 ◽  
Author(s):  
Young-Wook Kim ◽  
Shin-Han Kim ◽  
In-Hyuck Song ◽  
Hai-Doo Kim ◽  
Chul B. Park
Keyword(s):  
Silicon Carbide ◽  
Carbothermal Reduction ◽  
Open Cell ◽  
Carbide Ceramics ◽  
Silicon Carbide Ceramics

scholarly journals Optimal preparation of high-entropy boride-silicon carbide ceramics

2020 ◽  
Author(s):  
Yan Zhang ◽  
Shi-Kuan Sun ◽  
Wei-Ming Guo ◽  
Liang Xu ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Carbothermal Reduction ◽  
Powder Processing ◽  
Full Density ◽  
High Entropy ◽  
Sic Ceramics ◽  
Reduction Methods ◽  
Borothermal Reduction ◽  
Carbide Ceramics ◽  
Silicon Carbide Ceramics

Abstract High-entropy boride-silicon carbide (HEB-SiC) ceramics were fabricated by using boride-based powders prepared from borothermal and boro/carbothermal reduction methods. The effects of processing routes (borothermal reduction and boro/carbothermal reduction) of HEB powders were examined. HEB-SiC ceramics with nearly relatively full density (>98%) were prepared by spark plasma sintering at 2000oC. It was demonstrated that the addition of SiC led to slightly coarsening of the microstructure. The HEB-SiC ceramics prepared from boro/carbothermal reduction powders showed the fine-grained microstructure and higher Vickers’ hardness but lower fracture toughness values as compared with the same composition prepared from borothermal reduction powders. These results indicated that the selection of the powder processing method and the addition of SiC phase could contribute to the optimal preparation of high-entropy boride-based ceramics.

scholarly journals Optimal preparation of high-entropy boride-silicon carbide ceramics

2020 ◽  
Author(s):  
Yan Zhang ◽  
Shi-Kuan Sun ◽  
Wei-Ming Guo ◽  
Liang Xu ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Carbothermal Reduction ◽  
Powder Processing ◽  
High Entropy ◽  
Fine Grained ◽  
Sic Ceramics ◽  
Reduction Methods ◽  
Borothermal Reduction ◽  
Carbide Ceramics ◽  
Silicon Carbide Ceramics

Abstract High-entropy boride-silicon carbide (HEB-SiC) ceramics were fabricated using boride-based powders prepared from borothermal and boro/carbothermal reduction methods. The effects of processing routes (borothermal reduction and boro/carbothermal reduction) on the HEB powders were examined. HEB-SiC ceramics with > 98% theoretical density were prepared by spark plasma sintering at 2000 °C. It was demonstrated that the addition of SiC led to slight coarsening of the microstructure. The HEB-SiC ceramics prepared from boro/carbothermal reduction powders showed a fine-grained microstructure and higher Vickers’ hardness but lower fracture toughness value as compared with the same composition prepared from borothermal reduction powders. These results indicated that the selection of the powder processing method and the addition of SiC phase could contribute to the optimal preparation of high-entropy boride-based ceramics.

scholarly journals Optimal preparation of high-entropy boride-silicon carbide ceramics

2020 ◽  
Author(s):  
Yan Zhang ◽  
Shi-Kuan Sun ◽  
Wei-Ming Guo ◽  
Liang Xu ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Carbothermal Reduction ◽  
Powder Processing ◽  
Full Density ◽  
High Entropy ◽  
Sic Ceramics ◽  
Reduction Methods ◽  
Borothermal Reduction ◽  
Carbide Ceramics ◽  
Silicon Carbide Ceramics

Abstract High-entropy boride-silicon carbide (HEB-SiC) ceramics were fabricated by using boride-based powders prepared from borothermal and boro/carbothermal reduction methods. The effects of processing routes (borothermal reduction and boro/carbothermal reduction) of HEB powders were examined. HEB-SiC ceramics with nearly relatively full density (>98%) were prepared by spark plasma sintering at 2000 °C. It was demonstrated that the addition of SiC led to slightly coarsening of the microstructure. The HEB-SiC ceramics prepared from boro/carbothermal reduction powders showed the fine-grained microstructure and higher Vickers’ hardness but lower fracture toughness values as compared with the same composition prepared from borothermal reduction powders. These results indicated that the selection of the powder processing method and the addition of SiC phase could contribute to the optimal preparation of high-entropy boride-based ceramics.

scholarly journals Optimal Preparation of High-entropy Boride-silicon Carbide Ceramics

2020 ◽  
Author(s):  
Yan Zhang ◽  
Shi-Kuan Sun ◽  
Wei-Ming Guo ◽  
Liang Xu ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Carbothermal Reduction ◽  
Powder Processing ◽  
Full Density ◽  
High Entropy ◽  
Sic Ceramics ◽  
Reduction Methods ◽  
Borothermal Reduction ◽  
Carbide Ceramics ◽  
Silicon Carbide Ceramics

Abstract High-entropy boride-silicon carbide (HEB-SiC) ceramics were fabricated by using boride-based powders prepared from borothermal and boro/carbothermal reduction methods. The effects of processing routes of HEB powders were examined between borothermal reduction and boro/carbothermal reduction. HEB-SiC ceramics with nearly relatively full density (>98%) were prepared after spark plasma sintering at 2000oC. It was demonstrated that the addition of SiC led to the slightly microstructure coarsening. The HEB-SiC ceramics prepared from boro/carbothermal reduction powders showed the fine-grained microstructure and higher Vickers’ hardness but lower fracture toughness values as compared with the same composition prepared from borothermal reduction powders. These results indicated that the selection of the powder processing method and the addition of SiC phase could contribute to the optimal preparation of high-entropy boride based ceramics.

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