PP-029 Study of radionuclide impurities in 18f-metil-choline: Setup of the measurement geometry for high purity germanium gamma ray spectrometer

2016 ◽  
Vol 23 (Suppl 1) ◽  
pp. A207.1-A207
Author(s):  
D Saetta ◽  
A D’Arpino ◽  
A Rongoni ◽  
P Sabatini ◽  
S Beneventi ◽  
...  
2002 ◽  
Vol 30 (8) ◽  
pp. 1927-1931 ◽  
Author(s):  
M.N. Kobayashi ◽  
N. Hasebe ◽  
T. Miyachi ◽  
T. Doke ◽  
J. Kikuchi ◽  
...  

2019 ◽  
Vol 322 (3) ◽  
pp. 1331-1339
Author(s):  
Jerzy W. Mietelski

Abstract The paper presents the detection of background neutrons using the 558.4 keV gamma line emitted from excited 114Cd nuclei after neutron induced processes. Stable cadmium and 60 L water moderator were placed inside low background shield of high purity germanium (HPGe) based spectrometer. The method was applied to study diurnal mean variation of background neutron flux. For this purpose 1 h gamma background spectra of modified HPGe spectrometer were collected subsequently for 50.5 days and then summed in 24-h-cycle. Results for the 558.4 keV line are presented along with those of main background lines. The total gamma-ray spectrum was also analysed and results are presented and discussed. No cyclic structure was noticed for all examited lines but 2223 keV, for which some day-night effect is suggested to exist. Test of another moderator made of 108 kg of graphite was done, but the results obtained with water are more promising.


1993 ◽  
Vol 302 ◽  
Author(s):  
L.S. Darken ◽  
C. E. Cox

ABSTRACTHigh-purity germanium (HPGe) for gamma-ray spectroscopy is a mature technology that continues to evolve. Detector size is continually increasing, allowing efficient detection of higher energy gamma rays and improving the count rate and minimum detectable activity for lower energy gamma rays. For low-energy X rays, entrance window thicknesses have been reduced to where they are comparable to those in Si(Li) detectors. While some limits to HPGe technology are set by intrinsic properties, the frontiers have historically been determined by the level of control over extrinsic properties. The point defects responsible for hole trapping are considered in terms of the “standard level” model for hole capture. This model originates in the observation that the magnitude and temperature dependence of the cross section for hole capture at many acceptors in germanium is exactly that obtained if all incident s-wave holes were captured. That is, the capture rate is apparently limited by the arrival rate of holes that can make an angular-momentum-conserving transition to a s ground state. This model can also be generalized to other materials, where it may serve as an upper limit for direct capture into the ground state for either electrons or holes. The capture cross section for standard levels σS.L. is given bywhere g is the degeneracy of the ground state of the center after capture, divided by the degeneracy before capture. Mc is the number of equivalent extrema in the band structure for the carrier being captured, mo is the electronic mass, m* is the effective mass, and T is the temperature in degrees Kelvin.


2012 ◽  
Vol 27 (1) ◽  
pp. 13-19 ◽  
Author(s):  
Elio Tomarchio

The radionuclide purity of a radiopharmaceutical product is usually measured by gamma-ray spectrometry with various measurement geometries. The importance of this test is that the radionuclide impurities, if present, result in an increase in the radiation dose to the patient without contributing to diagnostic information and in some cases may also interfere with the marking molecules and affect the proper conduct of diagnostic examination. In this work, gamma-ray spectrometry is used to determine the amounts of impurities by adopting as measurement geometry the same bottle containing eluted or prepared radiopharmaceuticals. In addition to high-purity germanium semiconductor detectors, the usefulness of NaI(Tl) and LaBr3(Ce) scintillators in routine operation is also examined. For the latter detectors, an evaluation of the minimum detectable activity was carried out and compared with the activity limits established by the regulation rules. The main cases considered are related to the first elution of 99Mo-99mTc generators and samples of 18F-FDG (fluoro-deoxy-glucose) to be used for positron emission tomography diagnostics.


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