Nanoscale Mapping of Electrochemical Interfaces Using Three Dimensional Atom Probe Tomography

2009 ◽  
Keyword(s):  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe ◽  
Electrochemical Interfaces

scholarly journals High-Accuracy Sample Preparation for Three Dimensional Atom Probe Tomography Using Orthogonal Column Layout FIB-SEM and its STEM function

2018 ◽  
Vol 24 (S1) ◽  
pp. 830-831
Author(s):  
Miki Tsuchiya ◽  
Yoshihisa Orai ◽  
Takahiro Sato ◽  
Xin Man ◽  
Junichi Katane ◽  
...  
Keyword(s):  
Sample Preparation ◽  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe ◽  
High Accuracy

Three-Dimensional Chemical Mapping of a Single Protein in the Hydrated State with Atom Probe Tomography

2020 ◽  
Vol 92 (7) ◽  
pp. 5168-5177 ◽  
Author(s):  
Shi Qiu ◽  
Changxi Zheng ◽  
Vivek Garg ◽  
Yu Chen ◽  
Gediminas Gervinskas ◽  
...  
Keyword(s):  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe ◽  
Chemical Mapping ◽  
Single Protein

Three-dimensional doping and diffusion in nano scaled devices as studied by atom probe tomography

2013 ◽  
Vol 24 (27) ◽  
pp. 275705 ◽  
Author(s):  
Ajay Kumar Kambham ◽  
Arul Kumar ◽  
Antonios Florakis ◽  
Wilfried Vandervorst
Keyword(s):  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe ◽  
And Diffusion

Three-Dimensional Characterization of Deuterium Implanted in Silicon Using Atom Probe Tomography

2013 ◽  
Vol 6 (6) ◽  
pp. 066602 ◽  
Author(s):  
Hisashi Takamizawa ◽  
Katsuya Hoshi ◽  
Yasuo Shimizu ◽  
Fumiko Yano ◽  
Koji Inoue ◽  
...  
Keyword(s):  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe

scholarly journals Atom Probe Analysis of Ex Situ Gas-Charged Stable Hydrides

2017 ◽  
Vol 23 (2) ◽  
pp. 307-313 ◽  
Author(s):  
Daniel Haley ◽  
Paul A. J. Bagot ◽  
Michael P. Moody
Keyword(s):  
Atom Probe Tomography ◽  
Three Dimensional ◽  
Atom Probe ◽  
Atomic Scale ◽  
Ex Situ ◽  
Native Oxide ◽  
Probe Analysis ◽  
Atom Probe Tomography Analysis ◽  
Hydrogen Analysis ◽  
Atom Probe Analysis

AbstractIn this work, we report on the atom probe tomography analysis of two metallic hydrides formed by pressurized charging using an ex situ hydrogen charging cell, in the pressure range of 200–500 kPa (2–5 bar). Specifically we report on the deuterium charging of Pd/Rh and V systems. Using this ex situ system, we demonstrate the successful loading and subsequent atom probe analysis of deuterium within a Pd/Rh alloy, and demonstrate that deuterium is likely present within the oxide–metal interface of a native oxide formed on vanadium. Through these experiments, we demonstrate the feasibility of ex situ hydrogen analysis for hydrides via atom probe tomography, and thus a practical route to three-dimensional imaging of hydrogen in hydrides at the atomic scale.

Clustering and Local Magnification Effects in Atom Probe Tomography: A Statistical Approach

2010 ◽  
Vol 16 (5) ◽  
pp. 643-648 ◽  
Author(s):  
Thomas Philippe ◽  
Maria Gruber ◽  
François Vurpillot ◽  
D. Blavette
Keyword(s):  
Experimental Data ◽  
Atom Probe Tomography ◽  
Statistical Approach ◽  
Nearest Neighbor ◽  
Three Dimensional ◽  
Atom Probe ◽  
Quantitative Composition ◽  
Second Phase ◽  
Real Experimental Data ◽  
Open Issues

AbstractLocal magnification effects and trajectory overlaps related to the presence of a second phase (clusters) are key problems and still open issues in the assessment of quantitative composition data in three-dimensional atom probe tomography (APT) particularly for tiny solute-enriched clusters. A model based on the distribution of distance of first nearest neighbor atoms has been developed to exhibit the variations in the apparent atomic density in reconstructed volumes and to correct compositions that are biased by local magnification effects. This model was applied to both simulated APT reconstructions and real experimental data and shows an excellent agreement with the expected composition of clusters.

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