Anomalies in the analytical determination of water in epidote

Author(s):  
A. F. Smethurst

Numerous veins and veinlets of epidosite traverse the crystalline schists and associated igneous rocks of the Malvern complex. They art fine-grained, compact rocks, of uniform texture and pale greenish-yellow colour, and vary in composition from almost pure epidote to mixtures of epidote with small quantities of quartz, sphene, sericitic mica, apatite, and, in almost insignificant amount, albite.Analytical investigation of these rocks revealed the fact that the epidote they contain holds its water more tenaciously than has hitherto been suspected : the determination of water-content by the methods usually applied to the analysis of rocks and minerals gave results which were so seriously low as to suggest that the mineral was essentially anhydrous. Though more drastic methods increased the yield considerably, they failed to liberate more than about 75 % of the amount of water which, theoretically, should be present.

1941 ◽  
Vol 78 (1) ◽  
pp. 45-61 ◽  
Author(s):  
W. D. Urry ◽  
Arthur Holmes

The helium method of determining the ages of fine-grained basic igneous rocks has now been so far developed as to be applicable to various geological and petrological problems, particularly where geological periods are involved, as in the problem here discussed. For details of the history of this development up to the beginning of 1937 reference may be made to Holmes, 1931; Urry, 1933; Lane and Urry, 1935; Urry, 1936 (b); Holmes and Paneth, 1936; and Holmes, 1937. During 1937 it was found that many of the helium-ratios on which the ‘helium’ time-scale had been based were too high, because of a previously unsuspected error in radium determination due to reliance having being placed on a radium standard which was seriously at fault. To clear up this embarrassing situation an immediate effort was made by several investigators in collaboration, and the first fruits of their work have recently become available (Evans, Goodman, Keevil, Lane, and Urry, 1939).


2020 ◽  
Vol 50 (5) ◽  
pp. 347-350
Author(s):  
G. M. Druzhinin ◽  
N. B. Loshkarev ◽  
E. D. Solntseva ◽  
I. M. Khammatov

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