scholarly journals Intramolecular Interaction between Hydroxyl Group and π-Electrons. XI. High Resolution Proton Magnetic Resonance Spectra of Tertiary Alcohols Having π-Electrons

1960 ◽  
Vol 33 (11) ◽  
pp. 1632-1633 ◽  
Author(s):  
Michinori Oki ◽  
Hiizu Iwamura
1972 ◽  
Vol 55 (5) ◽  
pp. 1101-1103
Author(s):  
K D Bartle

Abstract Mass spectrometry allows the number of chlorine atoms per polychlorobiphenyl molecule to be determined but not the positions of substitution. A method of identifying PCB components from high resolution proton magnetic resonance spectra is illustrated by application to 2,5,2′,5′-tetrachloro- and 2,3,4,2′,4′,- 5′-hexachlorobiphenyls separated by gas chromatography from a commercial PCB mixture.


1961 ◽  
Vol 14 (1) ◽  
pp. 64 ◽  
Author(s):  
RJ Abraham ◽  
HJ Bernstein

The high resolution proton magnetic resonance spectra of himgravine and himbacine have been obtained in CHCl3 solution at 60 Mc/s. The spectra are consistent with only one of the two possible structures proposed. Other information with regard to relative orientation of groups within the molecule has also been obtained.


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