Darstellung und Kristallstruktur von (n-Bu4N)[ReBr5Py] / Synthesis and Crystal Structure of (n-Bu4N)[ReBr5Py]
2000 ◽
Vol 55
(6)
◽
pp. 484-486
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Keyword(s):
By reaction of (n-Bu4N)2[ReBr6] with pyridine and (n-Bu4N)BH4 in dichloromethane various bromo-pyridine-rhenium(III) complexes are formed which can be separated by chromatography. Electrochemical oxidation of (n-Bu4N)2[ReBr5Py] leads to (n-Bu4N)[ReBr5Py]. X-ray structure determination on a single crystal has been performed of (n-Bu4N)[ReBr5Py] (monoclinic, space group P21/n a = 11,248(5), b = 17,192(5), c = 15,206(5) Å, β = 97,600(5)°, Z = 4).
1998 ◽
Vol 53
(11)
◽
pp. 1335-1337
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1993 ◽
Vol 48
(7)
◽
pp. 1009-1012
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1988 ◽
Vol 43
(2)
◽
pp. 135-137
◽
2006 ◽
Vol 61
(10)
◽
pp. 1205-1208
◽
2015 ◽
Vol 70
(3)
◽
pp. 161-164
◽
Keyword(s):
1981 ◽
Vol 36
(10)
◽
pp. 1208-1210
◽
2015 ◽
Vol 70
(3)
◽
pp. 191-196
◽
2002 ◽
Vol 57
(1)
◽
pp. 43-46
◽
Keyword(s):