Anodic stripping voltammetric determination of uranium at a thin palladium film-aluminum electrode: Analysis of some uranium mineral ores

2010 ◽  
Vol 98 (4) ◽  
Author(s):  
M. H. Pournaghi-Azar ◽  
H. Dastangoo ◽  
R. Fadakar bajeh baj
2013 ◽  
Vol 104 ◽  
pp. 148-161 ◽  
Author(s):  
Silvia Illuminati ◽  
Anna Annibaldi ◽  
Cristina Truzzi ◽  
Carolina Finale ◽  
Giuseppe Scarponi

Proceedings ◽  
2018 ◽  
Vol 2 (13) ◽  
pp. 1518
Author(s):  
Maria Tsetsoni ◽  
Eleni Roditi ◽  
Christos Kokkinos ◽  
Anastasios Economou

In this work, a microfabricated Au-film sensor was designed and fabricated for thevoltammmetric determination of Hg(II). The electrode was fabricated on a silicon chip with astandard microengineering approach utilizing photolithography for patterning the electrode shapeand sputtering for deposition of thin Cr and Au films on the surface of the sensors. The sensorswere used for the determination of trace Hg(II) with anodic stripping voltammetry (ASV): initiallyHg(II) in the sample was accumulated on the Au working electrode surface by reduction andformation of an Au(Hg) amalgam followed by oxidation of the preconcentrated metallic Hg using asquare wave voltammetric scan. The limit of detection was 1.5μgL−1 and the coefficient of variationof 10 consecutive measurements was 3.1%.


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