Development of Plasma-assisted Synthesis Techniques for Carbon Nanotubes

2015 ◽  
Vol 135 (3) ◽  
pp. 148-150
Author(s):  
Yoshiyuki SUDA
2019 ◽  
pp. 81-106
Author(s):  
Saumya Shalu ◽  
Kakoli Dasgupta ◽  
Anuradha Kumari ◽  
Barnali Dasgupta Ghosh

2021 ◽  
Author(s):  
Syed Awais Rouf ◽  
Zahid Usman ◽  
Hafiz Tariq Masood ◽  
Abdul Mannan Majeed ◽  
Mudassira Sarwar ◽  
...  

In this chapter, we will evaluate the synthesis and purification of carbon nanotubes. Carbon nanotubes are cylindrical molecules that consists of graphene (rolled up of a single-layer carbon atom). A wide variety of synthesis techniques such as arc discharge synthesis, laser ablation of graphite/laser vaporization synthesis method, chemical vapor deposition (CVD), high pressure carbon monoxide synthesis and flame synthesis techniques, have been implemented to grow single and multi-walled carbon nanotubes for technological applications. All of the above methods exploit transition metals, like iron, cobalt, and nickel, as a catalyst. There are number of methods (filtering, chromatography and centrifugation) used to purify the carbon nanotubes, but the degree of purity remained questionable in these methods. In order to enhance the purification extent, alternate techniques such as Gas phase purification, Liquid phase purification and Purification by Intercalation are introduced. Here we will discuss the advantages and disadvantages of these purification routes. It will help researchers in selecting appropriate and effective method for synthesis and purification of carbon nanotubes.


Author(s):  
Jun Jiao

HREM studies of the carbonaceous material deposited on the cathode of a Huffman-Krätschmer arc reactor have shown a rich variety of multiple-walled nano-clusters of different shapes and forms. The preparation of the samples, as well as the variety of cluster shapes, including triangular, rhombohedral and pentagonal projections, are described elsewhere.The close registry imposed on the nanotubes, focuses attention on the cluster growth mechanism. The strict parallelism in the graphitic separation of the tube walls is maintained through changes of form and size, often leading to 180° turns, and accommodating neighboring clusters and defects. Iijima et. al. have proposed a growth scheme in terms of pentagonal and heptagonal defects and their combinations in a hexagonal graphitic matrix, the first bending the surface inward, and the second outward. We report here HREM observations that support Iijima’s suggestions, and add some new features that refine the interpretation of the growth mechanism. The structural elements of our observations are briefly summarized in the following four micrographs, taken in a Hitachi H-8100 TEM operating at an accelerating voltage of 200 kV and with a point-to-point resolution of 0.20 nm.


Nature China ◽  
2007 ◽  
Author(s):  
Rachel Pei Chin Won
Keyword(s):  

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