scholarly journals Overview of sorption analysis capabilities for meso- and microporous zeolites nanomaterials

2021 ◽  
Vol 8 (3) ◽  
pp. 20210302
Author(s):  
S. Tokmeilova ◽  
E. V. Maraeva

In this paper we consider the main application features of the thermal desorption method of inert gases, implemented on the Sorbi MS (Meta, Russia) device, for the analysis of meso- and microporous materials. Recommendations on the choice of measurement modes for stable operation of the Sorbi MS device are offered (including recommendations on mass, sample preparation mode). The article presents the results of the micropores analysis by the t-plot and Sing method.

2012 ◽  
Vol 10 (5) ◽  
pp. 1565-1573 ◽  
Author(s):  
Pavel Coufalík ◽  
Pavel Krásenský ◽  
Marek Dosbaba ◽  
Josef Komárek

AbstractMercury forms in contaminated environmental samples were studied by means of sequential extraction and thermal desorption from the solid phase. The sequential extraction procedure involved the following fractions: water soluble mercury, mercury extracted in acidic conditions, mercury bound to humic substances, elemental Hg and mercury bound to complexes, HgS, and residual mercury. In addition to sequential extraction, the distribution of mercury species as a function of soil particles size was studied. The thermal desorption method is based on the thermal decomposition or desorption of Hg compounds at different temperatures. The following four species were observed: Hg0, HgCl2, HgS and Hg(II) bound to humic acids. The Hg release curves from artificial soils and real samples were obtained and their applicability to the speciation analysis was considered.


1992 ◽  
Vol 37 (6) ◽  
pp. 1029-1031 ◽  
Author(s):  
Yoshio Takasu ◽  
Kohji Tsukada ◽  
Katsunori Nishimura ◽  
Tadao Hiromine ◽  
Kiyochika Yahikozawa

1995 ◽  
Vol 34 (Part 1, No. 9A) ◽  
pp. 5049-5053 ◽  
Author(s):  
Shigeru Imai ◽  
Takeo Haga ◽  
Osamu Matsuzaki ◽  
Takeo Hattori ◽  
Masakiyo Matsumura

1966 ◽  
Vol 9 (3) ◽  
pp. 112-114 ◽  
Author(s):  
E. V. Kornelsen ◽  
M. K. Sinha

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