scholarly journals Comparing plastic syringes and disposable columns to extract n-alkanes in forage and concentrate feeds

2010 ◽  
Vol 40 (8) ◽  
pp. 1844-1847 ◽  
Author(s):  
Dimas Estrasulas de Oliveira ◽  
Luis Orlindo Tedeschi

Saturated aliphatic hydrocarbons (n-alkanes) were extracted from feed, orts, and bovine fecal samples using disposable, plastic 5mL-syringes as an alternative material to disposable columns, which are normally used in the liquid-solid extraction phase of n-alkanes. For both methods, the n-alkane extracts (carbon chain length between 31 and 36 atoms) were identified using gas chromatography. The linear regression between methods were: 1) feces: column Alkane=2.63+0.92×syringeAlkane [r²=0.94, square root of the mean square error (RMSE)=13.7mg kg-1, n=30] from which the intercept and the slope did not simultaneously differ from zero and unity (P>0.05), respectively; 2) feeds: column Alkane=0.36+1.12×syringeAlkane (r²=0.85, RMSE=1.9mg kg-1, n=21) from which the intercept and the slope did not simultaneously differ from zero and unity (P>0.05), respectively; 3) orts: column Alkane=0.49+0.92×syringeAlkane (r²=0.98, RMSE=1.2mg kg-1, n=15) from which the intercept and the slope did not simultaneously differ from zero and unity (P>0.05), respectively. Materials with low concentration of n-alkanes may affect the values obtained in both methods. These results suggested that disposable plastic syringes might be a viable alternative to columns thus, reducing analytical costs.

Sensors ◽  
2021 ◽  
Vol 21 (5) ◽  
pp. 1631
Author(s):  
Bruno Guilherme Martini ◽  
Gilson Augusto Helfer ◽  
Jorge Luis Victória Barbosa ◽  
Regina Célia Espinosa Modolo ◽  
Marcio Rosa da Silva ◽  
...  

The application of ubiquitous computing has increased in recent years, especially due to the development of technologies such as mobile computing, more accurate sensors, and specific protocols for the Internet of Things (IoT). One of the trends in this area of research is the use of context awareness. In agriculture, the context involves the environment, for example, the conditions found inside a greenhouse. Recently, a series of studies have proposed the use of sensors to monitor production and/or the use of cameras to obtain information about cultivation, providing data, reminders, and alerts to farmers. This article proposes a computational model for indoor agriculture called IndoorPlant. The model uses the analysis of context histories to provide intelligent generic services, such as predicting productivity, indicating problems that cultivation may suffer, and giving suggestions for improvements in greenhouse parameters. IndoorPlant was tested in three scenarios of the daily life of farmers with hydroponic production data that were obtained during seven months of cultivation of radicchio, lettuce, and arugula. Finally, the article presents the results obtained through intelligent services that use context histories. The scenarios used services to recommend improvements in cultivation, profiles and, finally, prediction of the cultivation time of radicchio, lettuce, and arugula using the partial least squares (PLS) regression technique. The prediction results were relevant since the following values were obtained: 0.96 (R2, coefficient of determination), 1.06 (RMSEC, square root of the mean square error of calibration), and 1.94 (RMSECV, square root of the mean square error of cross validation) for radicchio; 0.95 (R2), 1.37 (RMSEC), and 3.31 (RMSECV) for lettuce; 0.93 (R2), 1.10 (RMSEC), and 1.89 (RMSECV) for arugula. Eight farmers with different functions on the farm filled out a survey based on the technology acceptance model (TAM). The results showed 92% acceptance regarding utility and 98% acceptance for ease of use.


2019 ◽  
pp. 08-16
Author(s):  
Nadine Danielle Coulibaly ◽  
Serge M.A. Somda ◽  
Césaire Tania Ouédraogo ◽  
Augustin N. Zéba ◽  
Hermann Sorgho ◽  
...  

We describe a simple method to validate data collected from a study using the deuterium oxide dose-to-the-mother technique for breastfeeding evaluation. We used human milk intake calculation spreadsheets (n=180). The calculation was performed by fitting the deuterium enrichment data to a model for water turnover in the mother and in the baby. We assumed that the validity of the results is as high as the square root mean square error (SRMSE) between calculated and fitted data is low. Based on the original spreadsheets that fitted well with the model (n=87), we developed a simple prediction of the SRMSE and we used it as cut-off to check, correct (by removing enrichment data) and validate or remove the other spreadsheets. We found a cut-off dependent on the measured enrichment (E_m) that was And the mean SRMSE (90%CI) of the fitted sheets was 23.37 mg.kg-1 (22.01 mg.kg-1, 24.73 mg.kg-1) with a maximum of 38.96 mg.kg-1. After correction we noticed that the number of enrichments removed per file varied from 1 to 4. We observed within the corrected spreadsheets a significant reduction (p≤0.0001, n=53) of the SRMSE (90%CI) from 49.78 mg.kg-1 (46.35 mg.kg-1, 53.20mg.kg-1) before correction to 25.88 mg.kg-1 (24.13 mg.kg-1, 27.64 mg.kg-1) after correction. We also observed that after correction, the mean difference (90%CI) of HM respectively non-HM that was 29.34 mg.kg-1 (21.71 mg.kg-1, 36.97 mg.kg-1) respectively 24.13 mg.kg-1 (17.4 mg.kg-1, 30.79 mg.kg-1) was strongly (p≤0.0001, n=53) different from zero. Therefore, the correction is very important to optimizing the results. Keywords: Breastfeeding; Deuterium; Excel spreadsheet; Square root mean square error; Validation


1978 ◽  
Vol 48 ◽  
pp. 227-228
Author(s):  
Y. Requième

In spite of important delays in the initial planning, the full automation of the Bordeaux meridian circle is progressing well and will be ready for regular observations by the middle of the next year. It is expected that the mean square error for one observation will be about ±0.”10 in the two coordinates for declinations up to 87°.


2018 ◽  
Vol 934 (4) ◽  
pp. 59-62
Author(s):  
V.I. Salnikov

The question of calculating the limiting values of residuals in geodesic constructions is considered in the case when the limiting value for measurement errors is assumed equal to 3m, ie ∆рred = 3m, where m is the mean square error of the measurement. Larger errors are rejected. At present, the limiting value for the residual is calculated by the formula 3m√n, where n is the number of measurements. The article draws attention to two contradictions between theory and practice arising from the use of this formula. First, the formula is derived from the classical law of the normal Gaussian distribution, and it is applied to the truncated law of the normal distribution. And, secondly, as shown in [1], when ∆рred = 2m, the sums of errors naturally take the value equal to ?pred, after which the number of errors in the sum starts anew. This article establishes its validity for ∆рred = 3m. A table of comparative values of the tolerances valid and recommended for more stringent ones is given. The article gives a graph of applied and recommended tolerances for ∆рred = 3m.


2011 ◽  
Vol 57 (7) ◽  
pp. 4622-4635 ◽  
Author(s):  
Bernhard G. Bodmann ◽  
Pankaj K. Singh

2021 ◽  
pp. 58-60
Author(s):  
Naziru Fadisanku Haruna ◽  
Ran Vijay Kumar Singh ◽  
Samsudeen Dahiru

In This paper a modied ratio-type estimator for nite population mean under stratied random sampling using single auxiliary variable has been proposed. The expression for mean square error and bias of the proposed estimator are derived up to the rst order of approximation. The expression for minimum mean square error of proposed estimator is also obtained. The mean square error the proposed estimator is compared with other existing estimators theoretically and condition are obtained under which proposed estimator performed better. A real life population data set has been considered to compare the efciency of the proposed estimator numerically.


Sign in / Sign up

Export Citation Format

Share Document