Abstract
A bismuth oxide based multi-component glass system, xH3BO3-yBi2O3-(1-x-y-δ)MO-δ·REO with MO=TiO2, BaO, ZnO, Fe2O3, etc., and lanthanum series based rare earth oxides (REO), for making downhole high-pressure and high-temperature (HPHT) electrical feedthrough package, has been developed using high-temperature melt-quenching and sintering technologies. By properly controlling phase structures in the material manufacturing processes, the obtained sealing materials have shown moisture-resistant properties in their monoclinic and tetragonal mixed phase structures, but strongly hydrophobic properties in their covalent bond tetragonal phase. The sealed electrical feedthrough packages have been evaluated under boiling water immersion and 200°C/30,000PSI water-fluid simulated downhole harsh environments. The post measurement has demonstrated to be greater than 1.0×1014 Ω electrical resistance. This paper will show that such a high-bonding-strength and high-insulation-strength sealing material could be used to seal electrical feedthroughs and connectors for 300°C/30,000PSI downhole and subsea wireline, logging while drilling (LWD), and measurement while drilling (MWD) tools' signal, data, and electrical power transmissions.