scholarly journals Особенности поведения доменной структуры кристаллов BaTiO-=SUB=-3-=/SUB=- в процессе термического нагрева и охлаждения-=SUP=-*-=/SUP=-

2018 ◽  
Vol 60 (4) ◽  
pp. 734
Author(s):  
Д.А. Киселев ◽  
Т.С. Ильина ◽  
М.Д. Малинкович ◽  
О.Н. Сергеева ◽  
Н.Н. Большакова ◽  
...  

AbstractThis paper presents the results of the study of the domain structure of barium titanate crystals in a wide temperature range including the Curie point ( T _C) using the polarization-optical method in the reflected light and the force microscopy of the piezoelectric response. It is shown that a new a–c domain structure forms during cyclic heating of the crystal above T _C and subsequent cooling to the ferroelectric phase. The role of uncompensated charges appeared on the crystal surface during the phase transition and their influence on the formation of the domain structure during cooling are discussed.

2000 ◽  
Vol 15 (12) ◽  
pp. 2814-2821 ◽  
Author(s):  
V. Bermúdez ◽  
A. Gil ◽  
L. Arizmendi ◽  
J. Colchero ◽  
A. M. Baró ◽  
...  

The domain structure of bulk periodically poled lithium niobate crystals were analyzed by different techniques. Images of topography, electrostatic force, and piezoelectric response were studied by scanning force microscopy. All these images showed the domain structure of the samples. The electrostatic force was always attractive pointing to a dielectric origin. The diffraction of a laser beam by the periodic structures was also observed, denoting a periodic change of refractive index. From the angle of diffraction the domain spatial frequency was directly obtained. The topographic profile of etched samples was studied by both scanning force and scanning electron microscopy.


1997 ◽  
Vol 55 (17) ◽  
pp. 11593-11603 ◽  
Author(s):  
R. P. Cowburn ◽  
J. Ferréand ◽  
J.-P. Jamet ◽  
S. J. Gray ◽  
J. A. C. Bland

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