Using X-ray computed tomography to measure local gas holdup in a stirred tank reactor

2006 ◽  
Author(s):  
Jason J. Ford
Author(s):  
Jason J. Ford ◽  
Theodore J. Heindel ◽  
Terrence C. Jensen

X-ray computed tomography (CT) is used to explore the differences in gas dispersion in a gas-sparged stirred-tank reactor (STR) for different operating conditions. X-ray CT imaging is completed for various impeller speeds and gas flow rates in a 0.21 m ID STR made out of acrylic and equipped with a nylon Rushton-type impeller. From the CT slices, major differences in local time-averaged gas holdup can be seen, depending on the operating condition. Completely dispersed conditions have a relatively uniform holdup profile while flooded conditions have an increase in gas holdup towards the center of the tank. The high resolution of the X-ray system allows for visualizing time-averaged gas flow details such as low gas holdup regions directly above the impeller region under certain operating conditions and recirculation regions behind the baffles.


2008 ◽  
Vol 63 (8) ◽  
pp. 2075-2085 ◽  
Author(s):  
Jason J. Ford ◽  
Theodore J. Heindel ◽  
Terrence C. Jensen ◽  
Joshua B. Drake

2012 ◽  
Vol 134 (8) ◽  
Author(s):  
Joshua B. Drake ◽  
Theodore J. Heindel

Fluidized beds are common equipment in many process industries. Knowledge of the hydrodynamics within a fluidized bed on the local scale is important for the improvement of scale-up and process efficiencies. This knowledge is lacking due to limited observational technologies at the local scale. This paper uses X-ray computed tomography (CT) imaging to describe the local time-average gas holdup differences of annular hydrodynamic structures that arise through axisymmetric annular flow in a 10.2 cm and 15.2 cm diameter cold flow fluidized bed. The aeration scheme used is similar to that provided by a porous plate and hydrodynamic results can be directly compared. Geldart type B glass bead, ground walnut shell, and crushed corncob particles were studied at various superficial gas velocities. Assuming axisymmetry, the local 3D time-average gas holdup data acquired through X-ray CT imaging was averaged over concentric annuli, resulting in a 2D annular and time-average gas holdup map. These gas holdup maps show that four different types of annular hydrodynamic structures occur in the fluidized beds of this study: zones of (1) aeration jetting, (2) bubble coalescence, (3) bubble rise, and (4) particle shear. Changes in the superficial gas velocities, bed diameters, and bed material densities display changes in these zones. The 2D gas holdup maps provide a benchmark that can be used by computational fluid dynamic (CFD) users for the direct comparisons of 2D models, assuming axisymmetric annular flow.


Author(s):  
Joshua B. Drake ◽  
Theodore J. Heindel

Characterizing the hydrodynamics in fluidized beds is important to many processes from producing biofuels to coating pharmaceuticals. X-ray computed tomography (CT) can quantify local time-averaged phase fractions in multiphase systems that are highly dynamic, like fluidized beds. This paper describes the calibration methods used to produced CT images of a 15.24 cm diameter fluidized bed, how in-house software used these CTs to calculate gas holdup, and how well multiple CTs of a dynamic fluidized bed produced repeatable results while varying bed material and superficial gas velocities. It was concluded there is a very high degree of repeatability using the calibration methods and in-house software developed.


2015 ◽  
Vol 138 (4) ◽  
Author(s):  
David R. Escudero ◽  
Theodore J. Heindel

Understanding the jetting phenomena near the gas distributor plate in a fluidized bed is important to gas–solid mixing, heat and mass transfer, and erosion to any bed internals, which can all affect the performance of the bed. Moreover, acoustic vibration in a fluidized bed can be used to enhance the fluidization quality of the particulate matter and influence the jetting behavior. Characterizing the jetting structure using X-ray computed tomography (CT) in a three-dimensional (3D) fluidized bed, with and without acoustic intervention, is the focus of this study. A 10.2 cm ID fluidized bed filled with glass beads and ground walnut shell, with material densities of 2500 kg/m3 and 1440 kg/m3, respectively, and particle sizes ranging between 212 and 600 μm, is used in these experiments. X-ray CT imaging is used to determine local time-average gas holdup. From this information, qualitative and quantitative characteristics of the hydrodynamic structure of the multiphase flow system are determined. Local time-average gas holdup images of the fluidized bed under acoustic intervention at a high superficial gas velocity show that jets produced near the aeration plate merge with other jets at a higher axial position of the bed compared to the no acoustic condition. Acoustic fluidized beds also have a fewer number of active jets than the no acoustic fluidized bed, which allowed for a more homogeneous gas holdup region deep in the bed. Hence, the acoustic presence has a significant effect on the jetting phenomena near the aeration plate in a fluidized bed.


Author(s):  
David R. Escudero ◽  
Theodore J. Heindel

Understanding the jetting phenomena near the gas distributor plate in a fluidized bed is important to gas-solids mixing, heat and mass transfer, and erosion on any bed internals, which can all affect the performance of the bed. Moreover, acoustic vibration in a fluidized bed can be used to enhance the fluidization quality of particulate matter. Characterizing the jetting structure using X-ray computed tomography in a 3D fluidized bed, with and without acoustic intervention, is completed in this study. A 10.2 cm ID fluidized bed filled with glass beads, with material density of 2500 kg/m3 and particles sizes ranging between 212–600 μm, is used in these experiments. X-ray computed tomography (CT) imaging is used to determine local time-average gas holdup. From this information, qualitative characteristics of the hydrodynamic structure of the multiphase flow system are determined. Local time-average gas holdup images of the fluidized bed under acoustic intervention at a high superficial gas velocity show that jets produced near the aeration plate merge with other jets at a higher axial position of the bed compared to the no acoustic condition. Acoustic fluidized beds also have a fewer number of active jets than the no acoustic fluidized bed, which allowed for a more homogeneous gas holdup region deep into the bed. Hence, the acoustic presence has a significant effect on the jetting phenomena near the distributor plate of the fluidized bed.


1999 ◽  
Vol 11 (1) ◽  
pp. 199-211
Author(s):  
J. M. Winter ◽  
R. E. Green ◽  
A. M. Waters ◽  
W. H. Green

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