Structural Phase State and Mechanical Properties of the Si-Al-N Coatings with Different Concentration Ratio of Al and Si

2015 ◽  
Vol 1085 ◽  
pp. 289-293 ◽  
Author(s):  
Viktor Sergeev ◽  
Marina V. Fedorischeva ◽  
Mark P. Kalashnikov ◽  
Irina A. Bozhko ◽  
Andrey V. Voronov ◽  
...  

The amorphous and nanocomposite coatings on the basis of Si-Al-N with different ratios of Al and Si concentrations were prepared by reactive magnetron sputtering method. Structural-phase state of coatings on the basis of Si-Al-N was investigated by TEM, SEM and X-ray analysis. Microhardness, modulus of elasticity, elastic recovery coefficient was determined by nanoindentation method.

2016 ◽  
Vol 683 ◽  
pp. 262-268 ◽  
Author(s):  
Irina A. Bozhko ◽  
Evgeniya V. Rybalko ◽  
Marina V. Fedorishcheva ◽  
Yury A. Vorobiev ◽  
Rais M. Magzhanov ◽  
...  

Nanocomposite coatings on the basis of Si-Al-N with different ratios of Al and Si concentrations were prepared using the reactive magnetron sputtering method. Internal stresses and structural-phase state of the two types of coatings was examined by X-ray analysis. The microhardness was measured by nanoindentation method. The microhardness, the elastic modulus and the coefficient of elastic recovery were determined. The optical transmission was measured for all types of samples.


2016 ◽  
Vol 685 ◽  
pp. 591-595
Author(s):  
Irina A. Bozhko ◽  
Evgeniya V. Rybalko ◽  
Mark P. Kalashnikov ◽  
Marina V. Fedorishcheva ◽  
Victor P. Sergeev

The transparent coatings on the basis of Al- Si- N system with high Al content and the opaque Al-Si-N with a low Al content were prepared by impulse magnetron sputtering method. Structural-phase state of the two types of coatings was examined by X-ray analysis. The microhardness was measured by nanoindentation method. The microhardness, the elastic modulus and the coefficient of elastic recovery were determined. Also the optical transmission was measured for all types of samples.


Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1638
Author(s):  
Nikolay Ababkov ◽  
Alexandr Smirnov ◽  
Vladimir Danilov ◽  
Lev Zuev ◽  
Natalya Popova ◽  
...  

The paper presents the results of the analysis of the microstructure, mechanical properties, acoustic and magnetic characteristics of the metal of pipelines that are part of heat and power equipment, after long-term operation, made of structural and heat-resistant steels in the zones of localization of plastic deformation. Samples of 0.2 С steel and 0.12С-1Сr-1Mo-1V steel were studied in the initial state, as well as after operation for 219 and 360 thousand hours, respectively. As a result of the studies carried out for each sample, the phase composition was determined (qualitatively and quantitatively), and the following parameters of the fine structure were calculated: volume fractions of structural components of steel (pearlite and ferrite), scalar and excess ± dislocation density, curvature-torsion of the crystal lattice χ, amplitude of internal stresses (shear stress and long-range stresses). All quantitative parameters of the structure are determined both in each structural component of steel, and in general for each sample. The structure of the metal of all specimens after deformation before the formation of zones of stable localization of deformations consists of a ferrite-pearlite mixture, and for specimens after operation before fracture only of unfragmented and fragmented ferrite. Ferrite, which occupies the bulk of the material, is present both unfragmented and fragmented. For all samples, the ratios ≥ , χ = χpl, σL ≥ σd were calculated, which indicate whether there is a danger of the initiation of microcracks in metal samples. For specimens without operation and after operation without damage in zones of stable localization of deformations, these conditions are met, and for specimens after operation until destruction, they are not met. It was found that the structural-phase state in the zones of localization of deformations has a direct effect on the characteristics of non-destructive tests. Thus, for all investigated samples, the values of such parameters as the delay time of the surface acoustic wave, the attenuation coefficient, the amplitude of the received signal, and the intensity of magnetic noise in the zones of deformation localization were established.


2015 ◽  
Vol 1085 ◽  
pp. 284-288 ◽  
Author(s):  
Viktor Sergeev ◽  
Mark P. Kalashnikov ◽  
Vasilii V. Neufeld

Results of surface modification of the VT-23 titanium alloy by high flux of copper ions with an energy of 2 keV and ion current density of 3.5 mA/cm2 was studied. The dependence of the microhardness and penetration depth of ion as function of duration of ion treatment was determined. Structural-phase state of ion-modified of the VT-23 titanium samples surface layer was investigated by TEM and SEM. Microhardness was researched by nanoindentation method.


2014 ◽  
Vol 1044-1045 ◽  
pp. 67-70
Author(s):  
Mazhyn Skakov ◽  
Gulnara Yerbolatova ◽  
Nurgamit Kantai ◽  
Michael Scheffler

It is shown that as a result of electrolytic plasma carburization is released from the solid solution carbides dispersed particles based alloy components, i.e. hardening occurs. Found that after processing the surface of the alloy samples 40CrNiAl modified form reinforced layers whose thickness depends on the time, temperature and processing of components of the electrolyte.


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