One Step Synthesis and Consolidation of Nanostructured ZrSi2-SiC Composite and its Mechanical Properties

2007 ◽  
Vol 124-126 ◽  
pp. 1149-1152
Author(s):  
In Jin Shon ◽  
Hyun Kuk Park ◽  
In Yong Ko ◽  
Jin Kook Yoon ◽  
Kyung Tae Hong
Keyword(s):  
Mechanical Properties ◽  
Combustion Synthesis ◽  
High Frequency ◽  
Combined Effects ◽  
Induced Current ◽  
Mechanical Pressure ◽  
Simultaneous Application ◽  
Average Grain Size ◽  
One Step ◽  
High Frequency Induction

Dense nanostructured ZrSi2-SiC composite was synthesized by high frequency induction heated combustion synthesis (HFIHCS) method within 1 minute in one step from powders of ZrC and 3Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of an induced current and mechanical pressure. Highly dense ZrSi2-SiC with relative density of up to 98% were produced under simultaneous application of a 60MPa pressure and the induced current. The average grain size and mechanical properties (hardness and fracture toughness) of the composite were investigated.

Simultaneous Synthesis and Consolidation of Nanostructured ZrB2–ZrO2 Composite

2020 ◽  
Vol 20 (7) ◽  
pp. 4349-4352
Author(s):  
Seong-Eun Kim ◽  
Jin-Kook Yoon ◽  
In-Jin Shon
Keyword(s):  
Mechanical Properties ◽  
Combustion Synthesis ◽  
High Frequency ◽  
Combined Effects ◽  
Induced Current ◽  
Mechanical Pressure ◽  
Simultaneous Application ◽  
Average Grain Size ◽  
One Step ◽  
Simultaneous Synthesis

A dense nanostructured 2ZrB2–ZrO2 composite was synthesized by the high-frequency inductionheated combustion synthesis (HFIHCS) method within 2 min in one step from mechanically activated powders of 2B2O3 and 3Zr. Simultaneous combustion synthesis and densification were accomplished under the combined effects of the induced current and mechanical pressure. A highly dense 2ZrB2–ZrO2 composite with relative density of up to 95.5% was produced under the simultaneous application of a pressure of 80 MPa and the induced current. The average grain size and mechanical properties (hardness and fracture toughness) of the composite were investigated.

Fabrication of Nanocrystalline TaSi2-SiC Composite by High Frequency Induction Heated Combustion Synthesis and Its Mechanical Properties.

2007 ◽  
Vol 534-536 ◽  
pp. 525-528 ◽  
Author(s):  
In Jin Shon ◽  
Dong Ki Kim ◽  
In Yong Ko ◽  
Jin Kook Yoon ◽  
Kyung Tae Hong
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Combustion Synthesis ◽  
High Frequency ◽  
Single Step ◽  
Combined Effects ◽  
Induced Current ◽  
Mechanical Pressure ◽  
Average Grain Size ◽  
High Frequency Induction

By the high frequency induction heated combustion synthesis (HFIHCS) method, dense nanostructured TaSi2-SiC composite was synthesized within 2 minutes and in a single step from powders of TaC and 3Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of an induced current and mechanical pressure. Highly dense TaSi2-SiC with relative density of up to 97% were produced under a 60MPa pressure and induced current. The average grain size and mechanical properties (hardness and fracture toughness) of the composite were investigated.

Simultaneous Synthesis and Densification of Nanostructured NbSi2-SiC-Si3N4 by Rapid Sintering

2010 ◽  
Vol 123-125 ◽  
pp. 209-212
Author(s):  
In Jin Shon ◽  
Hyun Su Kang ◽  
Soo Kyung Bae ◽  
In Yong Ko
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
High Frequency ◽  
Induced Current ◽  
Simultaneous Application ◽  
Average Grain Size ◽  
Rapid Sintering ◽  
One Step ◽  
Simultaneous Synthesis ◽  
High Frequency Induction

A dense nanostructured 5NbSi2-SiC-Si3N4 composite was synthesized by the high-frequency induction-heated combustion synthesis (HFIHCS) method within 1 minute in one step from mechanically activated powders of 4NbN, NbC and 14Si. A highly dense 5NbSi2-SiC-Si3N4 composite with relative density of up to 98% was produced under the simultaneous application of a pressure of 80 MPa and the induced current. The average grain size and mechanical properties (hardness and fracture toughness) of the composite were investigated.

Consolidation and Mechanical Properties of Nanostructured SiC from Mechanically Activated Powder by High-Frequency Induction-Heated Sintering

2010 ◽  
Vol 123-125 ◽  
pp. 635-638
Author(s):  
In Jin Shon ◽  
Hyun Su Kang ◽  
Na Ra Park ◽  
In Yong Ko
Keyword(s):  
Mechanical Properties ◽  
High Frequency ◽  
Sintering Behavior ◽  
Hard Material ◽  
Induced Current ◽  
Sintering Process ◽  
Simultaneous Application ◽  
Hard Materials ◽  
Rapid Sintering ◽  
High Frequency Induction

The rapid sintering of nanostuctured SiC hard materials was investigated with high-frequency induction heating sintering process. The advantage of this process is that it allows very quick densification to near theoretical density and prohibition of grain growth in nanostuctured materials. A dense nanostructured SiC hard material was produced with simultaneous application of 500 MPa pressure and induced current within 2 minutes. The effect of the ball milling times on the sintering behavior, grain size and mechanical properties of binderless SiC was investigated.

Properties and Rapid Consolidation of Nanostructured Fe3Al Compound by High Frequency Induction Heating

2010 ◽  
Vol 123-125 ◽  
pp. 759-762
Author(s):  
In Jin Shon ◽  
Tae Wan Kim ◽  
Jung Mann Doh ◽  
Jin Kook Yoon ◽  
Kwon Il Na ◽  
...  
Keyword(s):  
High Frequency ◽  
High Energy ◽  
Sintering Behavior ◽  
Combined Effects ◽  
Induced Current ◽  
Mechanical Pressure ◽  
Rapid Sintering ◽  
Energy Ball ◽  
Sintering Method ◽  
High Frequency Induction

A dense nanostuctured Fe3Al was consolidated by high frequency induction heated sintering method within 2 minutes from mechanically synthesized powders of Fe3Al and milled powders of 3Fe+Al. The consolidation was accomplished under the combined effects of a induced current and mechanical pressure. The grain size, sintering behavior and hardness of Fe3Al sintered from horizontally milled Fe+Al powders and high energy ball milled Fe3Al powder were compared. Keywords: Combustion synthesis; Nanomaterials; Mechanical properties; Rapid sintering

Simultaneous Synthesis and Consolidation of Nanostructured HfB2–SiC Composite

2021 ◽  
Vol 21 (7) ◽  
pp. 4011-4015
Author(s):  
Seong-Eun Kim ◽  
Jin-Kook Yoon ◽  
In-Jin Shon
Keyword(s):  
Fracture Toughness ◽  
Relative Density ◽  
Combustion Synthesis ◽  
Pulsed Current ◽  
Mechanical Pressure ◽  
Simultaneous Application ◽  
One Step ◽  
Simultaneous Synthesis ◽  
Short Time ◽  
Sintering Method

A dense nanostructured 2HfB2-SiC composite was simultaneously synthesized and consolidated by the pulsed current activated sintering method in one step within very short time (two minutes) from mechanically activated 2Hf, B4C and Si powders. Simultaneous combustion synthesis and consolidation were achieved through the combination of the effects of the pulsed current and mechanical pressure. A highly dense 2HfB2–SiC composite with 97.5% relative density was achieved under the simultaneous application of a pressure of 80 MPa and the pulsed current. The fracture toughness of the 2HfB2–SiC composite was higher than that of monolithic HfB2.

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