scholarly journals Accurate Determination of High Field Strength Elements (HFSE) in Geological Samples by ICP-MS Using an Improved Closed Digestion with Tartaric Acid as Matrix Modifier

2019 ◽  
Vol 40 (4) ◽  
pp. 113-121
Author(s):  
Huan Yang ◽  
Lanlan Jin ◽  
Xiuji Wang ◽  
Wenxia Liu ◽  
Shaowei Wu
Author(s):  
Bagai-ool Yu. Saryg-ool ◽  
Lidiya N. Bukreeva ◽  
Irina N. Myagkaya ◽  
Aleksandr V. Tolstov ◽  
Elena V. Lazareva ◽  
...  

Influence of sample pretreatment on the analysis of the high contents of rare earth (REE) and high field strength (HFSE) elements in geological samples by inductively coupled plasma atomic emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS) was studied. The rocks and rich ores of the Tomtor Nb-REE deposit were explored. Complete dissolution of the geological samples with a high content of “refractory” minerals has been achieved using fusion with a sodium peroxide. The results obtained by ICP-AES and ICP-MS after chemical dissolution are comparable with the results obtained by the XRF-SR without chemical pretreatment


RSC Advances ◽  
2019 ◽  
Vol 9 (56) ◽  
pp. 32435-32440 ◽  
Author(s):  
Rui Tong ◽  
Wei Guo

A simple, rapid, and reliable method based on slurry nebulisation inductively coupled plasma mass spectrometry (ICP-MS) was developed for the direct determination of four high field strength elements (HFSEs, namely, Nb, Ta, Zr, and Hf) in refractory silicate rocks.


2011 ◽  
Vol 26 (6) ◽  
pp. 1237 ◽  
Author(s):  
Yue-Heng Yang ◽  
Zhu-Yin Chu ◽  
Fu-Yuan Wu ◽  
Lie-Wen Xie ◽  
Jin-Hui Yang

2020 ◽  
Vol 35 (7) ◽  
pp. 1360-1367 ◽  
Author(s):  
Jianfeng Liu ◽  
Jiubin Chen ◽  
Ting Zhang ◽  
Yina Wang ◽  
Wei Yuan ◽  
...  

A new purification approach is reported for the highly precise and accurate determination of Sb isotope ratios in geological samples.


2016 ◽  
Vol 31 (8) ◽  
pp. 1673-1679 ◽  
Author(s):  
Ting Zhang ◽  
Lian Zhou ◽  
Lu Yang ◽  
Qian Wang ◽  
Lan-ping Feng ◽  
...  

A new MC-ICP-MS approach is reported for highly precise and accurate determination of the Ga isotope ratio in geological samples.


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