Oxygen Pressure Aging. Improved Equipment
Abstract Since the introduction of the oxygen pressure-aging test by Bierer and Davis, prevailing standard conditions for the test have been 70° C. (158° F.) and 300 pounds per square inch oxygen pressure. Various types of equipment have been used; usually the equipment has consisted of a pressure vessel immersed in a constant-temperature water bath to which is connected an oxygen supply. In the majority of instances the equipment has been difficult to operate and maintain for several reasons: Immersion of pressure vessels in a water bath made handling difficult. Corrosion was a continuous source of trouble, causing “freezing” of cover bolts and making it difficult to obtain a leakproof oxygen seal between cover and vessel. This caused loss of oxygen. Each time the pressure vessel was removed from the bath it was necessary to disconnect the oxygen supply and make the connection again when the test was started. This also caused loss of oxygen. If more than one pressure vessel was connected to the oxygen supply and a safety released, the entire oxygen supply was exhausted. The original pressure vessels were relatively large. Since the use of age resistors on a large scale, smaller units have been desirable in order to decrease migration of age resistors and eliminate erroneous results. Some of these operation difficulties were outlined by Ingmanson and Kemp, who also emphasized the importance of temperature control to obtain reproducible results. It is the purpose of this paper to describe an improved oxygen pressure installation which avoids some of these difficulties.