The effect of additional alloying elements on the decomposition of metastable beta titanium alloys during isothermal aging has received much attention for the past few years. Aluminum, which is an a-stabilizer, was shown to effectively retard the formation of ω-phase and accelerate 𝛂-nucleation. It was proposed by previous investigators that complete suppression of ω-phase in titanium alloys, with large amounts of the alloying elements, leads to the decomposition of ω-phase through an intermediate phase separation reaction. In the present studies, phase transformations in Ti-15w/oMo-3w/oAl were investigated using X-ray diffraction and transmission electron microscopy.