The OPCW Gas Chromatograph/Mass Spectrometer for On-Site Analysis. Instrumentation, AMDIS Software and Preparations for Use

Author(s):  
Mieczyslaw Sokolowski
Author(s):  
Takamitsu Iwaya ◽  
Shingo Akao ◽  
Kazushi Yamanaka ◽  
Tatsuhiro Okano ◽  
Nobuo Takeda ◽  
...  

Abstract For on-site analysis of surface materials on the moon, planets, and small bodies and for the monitoring of air quality in crewed spacecraft, we have developed a portable gas chromatograph (GC) equipped with a ball surface acoustic wave (SAW) sensor. In this study, we fabricated a 10 cm cube GC that implements the forward flush method using two metal micro-electro-mechanical-system (MEMS) columns coated with different stationary phases in microchannels fabricated by wet etching and diffusion bonding of stainless-steel plates. Using this GC, we succeeded in analyzing 10 kinds of gas within 10 min. In addition, for the application of the ball SAW GC on the ground, we also developed a palm-sized GC with a single metal capillary column and used it in the analysis of the headspace gas of sake. We showed that the ratio of peak areas differed among odorants depending on the brand and brewing process of sake.


2005 ◽  
Vol 47 (1) ◽  
pp. 74-77 ◽  
Author(s):  
Shigeru Suna ◽  
Fumihiko Jitsunari ◽  
Fumiyuki Asakawa ◽  
Tomohiro Hirao ◽  
Toshifumi Mannami ◽  
...  

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