Rapidly, highly yielded and green synthesis of dihydrotetrazolo[1,5‐ a ]pyrimidine derivatives in aqueous media using recoverable Pd (II) thiazole catalyst accelerated by ultrasonic: Computational studies

Author(s):  
Mahmoud Abd El Aleem Ali Ali El‐Remaily ◽  
Ahmed M. M. Soliman ◽  
Mohamed E. Khalifa ◽  
Nashwa M. El‐Metwaly ◽  
Amerah Alsoliemy ◽  
...  
2018 ◽  
Vol 9 (1) ◽  
pp. 101-108 ◽  
Author(s):  
Shubhangi J. Mane-Gavade ◽  
Sandip R. Sabale ◽  
Xiao-Ying Yu ◽  
Gurunath H. Nikam ◽  
Bhaskar V. Tamhankar

Introduction: Herein we report the green synthesis and characterization of silverreduced graphene oxide nanocomposites (Ag-rGO) using Acacia nilotica gum for the first time. Experimental: We demonstrate the Hg2+ ions sensing ability of the Ag-rGO nanocomposites form aqueous medium. The developed colorimetric sensor method is simple, fast and selective for the detection of Hg2+ ions in aqueous media in presence of other associated ions. A significant color change was noticed with naked eye upon Hg2+ addition. The color change was not observed for cations including Sr2+, Ni2+, Cd2+, Pb2+, Mg2+, Ca2+, Fe2+, Ba2+ and Mn2+indicating that only Hg2+ shows a strong interaction with Ag-rGO nanocomposites. Under the most suitable condition, the calibration plot (A0-A) against concentration of Hg2+ was linear in the range of 0.1-1.0 ppm with a correlation coefficient (R2) value 0.9998. Results & Conclusion The concentration of Hg2+ was quantitatively determined with the Limit of Detection (LOD) of 0.85 ppm. Also, this method shows excellent selectivity towards Hg2+ over nine other cations tested. Moreover, the method offers a new cost effective, rapid and simple approach for the detection of Hg2+ in water samples.


RSC Advances ◽  
2021 ◽  
Vol 11 (43) ◽  
pp. 26683-26686
Author(s):  
Md. Mahiuddin ◽  
Bungo Ochiai

Lemon juice effectively served as a reducing and capping agent for an easy, cost-effective, and green synthesis of crystalline bismuth nanoparticles (BiNPs) in basic aqueous media.


Author(s):  
Wei Zhang ◽  
Yi-jing Gao ◽  
Qiao-Jun Fang ◽  
Jin-kong Pan ◽  
Xin-Cheng Zhu ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-7 ◽  
Author(s):  
Harshita Sachdeva ◽  
Diksha Dwivedi ◽  
Rekha Saroj

Alum (KAl(SO4)2·12H2O) is an inexpensive, efficient, and nontoxic catalyst used for the synthesis of 2-[3-amino-5-methyl-5-(pyridin-3-yl)-1,5-dihydro-4H-1,2,4-triazol-4-yl]propanoic acid derivatives in aqueous media by the reaction of 3-acetyl pyridine(1), amino acids(2)/(6), and thiosemicarbazide(4)at 80°C. This methodology offers significant improvements for the synthesis of products with regards to the yield of products, simplicity in operation, and green aspects by avoiding toxic catalysts which uphold the motto of green chemistry. Synthesized compounds have been characterized by FT-IR,13C NMR, and1HNMR spectroscopy.


ChemInform ◽  
2007 ◽  
Vol 38 (36) ◽  
Author(s):  
Mazaahir Kidwai ◽  
Kavita Singhal ◽  
Shuchi Kukreja

2018 ◽  
Vol 67 ◽  
pp. 316-325 ◽  
Author(s):  
Kyung-Won Jung ◽  
Brian Hyun Choi ◽  
Seon Yong Lee ◽  
Kyu-Hong Ahn ◽  
Young Jae Lee

ChemInform ◽  
2006 ◽  
Vol 37 (17) ◽  
Author(s):  
Jing Yu ◽  
Hanqing Wang

RSC Advances ◽  
2015 ◽  
Vol 5 (9) ◽  
pp. 6578-6587 ◽  
Author(s):  
Balijapalli Umamahesh ◽  
Triveni Rajashekhar Mandlimath ◽  
Kulathu I. Sathiyanarayanan

The preparation of an eco-friendly, highly stable, reusable nano ZnAl2O4was used as an excellent catalyst for the pseudo four component synthesis of a library of fluorescent chromeno[2,3-d]pyrimidine derivatives.


Sign in / Sign up

Export Citation Format

Share Document