Controlled Synthesis of Well-Ordered Mesoporous Titania Films with Large Mesopores Templated by Spherical PS-b-PEO Micelles

2013 ◽  
Vol 2013 (19) ◽  
pp. 3286-3291 ◽  
Author(s):  
Xiangfen Jiang ◽  
Norihiro Suzuki ◽  
Bishnu Prasad Bastakoti ◽  
Wei-Jung Chen ◽  
Yu-Tzu Huang ◽  
...  
Keyword(s):  
Mesoporous Titania ◽  
Controlled Synthesis ◽  
Ordered Mesoporous ◽  
Large Mesopores ◽  
Titania Films

Exfoliated Graphene into Highly Ordered Mesoporous Titania Films: Highly Performing Nanocomposites from Integrated Processing

2013 ◽  
Vol 6 (2) ◽  
pp. 795-802 ◽  
Author(s):  
Luca Malfatti ◽  
Paolo Falcaro ◽  
Alessandra Pinna ◽  
Barbara Lasio ◽  
Maria F. Casula ◽  
...  
Keyword(s):  
Mesoporous Titania ◽  
Exfoliated Graphene ◽  
Ordered Mesoporous ◽  
Integrated Processing ◽  
Titania Films

Controlled Synthesis of Ordered Mesoporous Carbon-Cobalt Oxide Nanocomposites with Large Mesopores and Graphitic Walls

2016 ◽  
Vol 28 (21) ◽  
pp. 7773-7780 ◽  
Author(s):  
Zhengren Wang ◽  
Yongheng Zhu ◽  
Wei Luo ◽  
Yuan Ren ◽  
Xiaowei Cheng ◽  
...  
Keyword(s):  
Cobalt Oxide ◽  
Mesoporous Carbon ◽  
Ordered Mesoporous Carbon ◽  
Controlled Synthesis ◽  
Ordered Mesoporous ◽  
Large Mesopores

scholarly journals Spray Deposition Synthesis of Locally Ordered Mesoporous Polycrystalline Titania Films at Low Temperature

Molecules ◽  
2022 ◽  
Vol 27 (1) ◽  
pp. 303
Author(s):  
Gunnar Símonarson ◽  
Antiope Lotsari ◽  
Anders E. C. Palmqvist
Keyword(s):  
Low Temperature ◽  
Aging Time ◽  
Self Assembly ◽  
Spray Deposition ◽  
Spray Coating ◽  
Mesoporous Titania ◽  
Structure Directing Agent ◽  
Synthesis Time ◽  
Ordered Mesoporous ◽  
Titania Films

A low-temperature spray deposition synthesis was developed to prepare locally hexagonally ordered mesoporous titania films with polycrystalline anatase pore walls in an evaporation-induced self-assembly process. The titania film preparation procedure is conducted completely at temperatures below 50 °C. The effects of spray time, film thickness, synthesis time prior to spray deposition, and aging time at high relative humidity after deposition on the atomic arrangement and the mesoorder of the mesoporous titania were studied. We find the crystallite size to depend on both the synthesis time and aging time of the films, where longer times result in larger crystallites. Using the photocatalytic activity of titania, the structure-directing agent is removed with UV radiation at 43–46 °C. The capability of the prepared films to remove the polymer template increased with longer synthesis and aging times due to the increased crystallinity, which increases the photocatalytic efficiency of the titania films. However, with increasingly longer times, the crystallites grow too large for the mesoorder of the pores to be maintained. This work shows that a scalable spray coating method can be used to prepare locally ordered mesoporous polycrystalline titania films by judiciously tuning the synthesis parameters.

scholarly journals Ordered mesoporous titania from highly amphiphilic block copolymers: tuned solution conditions enable highly ordered morphologies and ultra-large mesopores

2015 ◽  
Vol 3 (21) ◽  
pp. 11478-11492 ◽  
Author(s):  
Morgan Stefik ◽  
Juho Song ◽  
Hiroaki Sai ◽  
Stefan Guldin ◽  
Patrick Boldrighini ◽  
...  
Keyword(s):  
Block Copolymers ◽  
Molar Mass ◽  
Amphiphilic Block Copolymers ◽  
Mesoporous Titania ◽  
High Molar Mass ◽  
Ordered Mesoporous ◽  
Titania Nanostructures ◽  
Large Mesopores ◽  
Triblock Terpolymers

Solubility guidelines enable the use of high molar mass block copolymers and ABC triblock terpolymers for the coassembly of titania nanostructures.

scholarly journals Thermal Conductivity of Ordered Mesoporous Titania Films Made from Nanocrystalline Building Blocks and Sol−Gel Reagents

2010 ◽  
Vol 114 (29) ◽  
pp. 12451-12458 ◽  
Author(s):  
Thomas Coquil ◽  
Christian Reitz ◽  
Torsten Brezesinski ◽  
E. Joseph Nemanick ◽  
Sarah H. Tolbert ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Sol Gel ◽  
Building Blocks ◽  
Mesoporous Titania ◽  
Ordered Mesoporous ◽  
Titania Films

Assembly of thin mesoporous titania films and their effects on the voltammetry of weakly adsorbing redox systems

2005 ◽  
Vol 579 (2) ◽  
pp. 267-275 ◽  
Author(s):  
Katy J. McKenzie ◽  
Pauline M. King ◽  
Frank Marken ◽  
Catherine E. Gardner ◽  
Julie V. Macpherson
Keyword(s):  
Mesoporous Titania ◽  
Redox Systems ◽  
Titania Films

scholarly journals Nano-sized blue spectral shift in sol–gel derived mesoporous titania films

2011 ◽  
Vol 61 (2) ◽  
pp. 355-361 ◽  
Author(s):  
P. Karasiński ◽  
E. Gondek ◽  
S. Drewniak ◽  
I. V. Kityk
Keyword(s):  
Sol Gel ◽  
Spectral Shift ◽  
Mesoporous Titania ◽  
Titania Films
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