Influence of the mode of introduction of a reactive element on the high temperature oxidation behavior of an alumina-forming alloy. Part III: The use of two stage oxidation experiments and in situ X-ray diffraction to understand the oxidation mechanisms

2006 ◽  
Vol 57 (6) ◽  
pp. 476-483 ◽  
Author(s):  
S. Chevalier ◽  
C. Issartel ◽  
R. Cueff ◽  
H. Buscaif ◽  
G. Strehl ◽  
...  
Author(s):  
Xin Zhang ◽  
Zehua Wang ◽  
Jinran Lin

AbstractFeCrBAlMo coating was deposited on an AISI 20 steel substrate by high velocity arc spraying (HVAS). Compared with FeCrBSiMo coating and pristine AISI 20 steel, the microstructure and high temperature oxidation behavior of FeCrBAlMo coating were investigated by optical microscopy, scanning electron microscopy, energy-dispersive spectroscopy and X-ray diffraction. Meanwhile, the bonding strength of the coatings was also measured. The results indicated that both coatings were composed of α(Fe,Cr) and Fe


2010 ◽  
Vol 105-106 ◽  
pp. 162-164
Author(s):  
Hong Bo Chen ◽  
Song He Meng

High temperature oxidation testing was carried out on hot-pressed ZrB2-SiC-graphite composite by using high electric current heating. The composites oxidation behavior was investigated, the temperature of oxidized specimens was above 2000°C. The results found that the UHTC composite was ruptured at oxidized temperature 2055°C. The microstructure of surface and cross-section of posttest samples were investigated by scanning electron microscopy along with energy and X-ray diffraction. The failure mechanism of rupture was also discussed.


2018 ◽  
Vol 921 ◽  
pp. 168-176
Author(s):  
Chang Hai Zhou ◽  
Rui Yun Pan ◽  
Hai Tao Ma

The oxidation behavior of Fe-20Ni alloy under compressive stress in air was studied at 800, 900 °C. The results examined by using scanning electron microscope (SEM) and X-ray diffraction (XRD) indicates that the oxide scales were consisted of an external scale and a subscale which has an intragranular scale (above 5 h at 800 °C and 900 °C) and an intergranular scale. Compared with the unstressed specimen, the growth kinetics of external scale was accelerated by an applied compressive stress. Besides, the compressive stress induced an increase in the growths of intragranular scale and intergranular scale formed on the specimens oxidized at 900 °C. However, the effect of compressive stress on the growth of intergranular scale and intragranular scale was not obvious in the case of 800°C. In addition, cracks developed in the subscale for the specimens oxidized under 2.5 MPa compressive stress when the oxidation time exceeded 20 h.


2002 ◽  
Vol 12 (6) ◽  
pp. 39-46
Author(s):  
R. Cueff ◽  
H. Buscail ◽  
E. Caudron ◽  
C. Issartel ◽  
S. Perrier ◽  
...  

2019 ◽  
Vol 141 (4) ◽  
Author(s):  
Grzegorz Moskal ◽  
Damian Migas ◽  
Dawid Niemiec ◽  
Agnieszka Tomaszewska

Cobalt-based γ–γ′ superalloys are novel heat-resistant materials suitable for high-temperature applications, such as components of the turbine engine. These alloys exhibit favorable strength and corrosion resistance at high temperatures owing to the γ–γ′ microstructure, analogous to that of Ni-based superalloys. The aim of this paper is to evaluate the oxidation behavior of basic Co-9Al-9W (at%) and new tungsten-free Co-10Al-5Mo-2Nb (at%) alloys at elevated temperatures. The investigation is concerned with thermogravimetric studies in the temperature range of 40–1200 °C. The oxidized surfaces after high temperature oxidation have been characterized using optical microscopy (OM), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and X-ray diffraction analysis (XRD).


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