Factor analysis of spectral data from chemical reactions

Author(s):  
G. Gauglitz ◽  
S. Weiß
2012 ◽  
Vol 67 (11-12) ◽  
pp. 580-586 ◽  
Author(s):  
Mohammad Aslam ◽  
Mohammed Ali ◽  
Rameshwar Dayal ◽  
Kalim Javed

Phytochemical investigations of the methanolic extract of the fruits of Peucedanum grande C. B. Clarke (Apiaceae) led to the identification of three coumarins and a naphthyl labdanoate diarabinoside characterized as 5-hydroxy-6-isopranyl coumarin (1), 5,6-furanocoumarin (2), 7-methoxy-5,6-furanocoumarin (3), and labdanyl-3α-ol-18-(3’’’-methoxy-2’’’- naphthyl-oate)-3α-L-arabinofuranosyl-(2’→1’’)-α-L-arabinofuranoside (4). The structures of these compounds were identified on the basis of spectral data analysis and chemical reactions. The methanolic extract and 4 showed nephroprotective activity against gentamicininduced nephrotoxicity in Wistar rats.


2011 ◽  
Vol 126 (2) ◽  
pp. 745-750 ◽  
Author(s):  
Yating Liu ◽  
Jian Deng ◽  
Lin An ◽  
Jun Liang ◽  
Fei Chen ◽  
...  

2002 ◽  
Vol 454 (1) ◽  
pp. 21-30 ◽  
Author(s):  
Zhong-Liang Zhu ◽  
Jun Xia ◽  
Jiang Zhang ◽  
Tong-Hua Li

1989 ◽  
Vol 67 (2) ◽  
pp. 275-278 ◽  
Author(s):  
Jairo Saez ◽  
Estella Fernandez ◽  
Akino Jossang ◽  
André Cavé ◽  
Adrien Cavé

Four new alkaloids, (−)-cordobine 1, (−)-monterine 2, (−)-granjine 3, and (−)-cordobimine 4 have been isolated from a Colombian Annonaceous plant, Crematosperma sp. Structures were elucidated from spectral data and chemical reactions. These alkaloids are the first 1R, 1′S bisbenzyltetrahydroisoquinolines including 8,7′ ether and 11,11′ biphenyl linkages. Keywords: Annonaceae, Crematosperma, alkaloids, biphenylbisbenzylisoquinolines.


2011 ◽  
Vol 66 (1-2) ◽  
pp. 17-23 ◽  
Author(s):  
Onkar Singh ◽  
Mohammed Ali ◽  
Nida Akhtar

Phytochemical investigations of the ethanolic extract of the seeds of Rhus coriaria L. (Anacardiaceae) led to the identification of four new xanthones, characterized as 2,3-dihydroxy- 7-methyl xanthone (1), 2,3,6-trihydroxy-7-hydroxymethylene xanthone-1-carboxylic acid (2), 2-methoxy-4-hydroxy-7-methyl-3-O-β-D-glucopyranosyl xanthone-1,8-dicarboxylic acid (4), and 2-hydroxy-7-hydroxymethylene xanthone-1,8-dicarboxylic acid 3-O-β-D-glucopyranosyl- (2’ → 3’’)-3’’-O-stigmast-5-ene (5), along with the known steroidal glucoside β-sitosterol-β-Dglucoside (3). The structures of the isolated compounds have been identifi ed on the basis of spectral data analysis and chemical reactions. All xanthones were active against Aspergillus flavus.


1973 ◽  
Vol 28 (7-8) ◽  
pp. 468-470 ◽  
Author(s):  
R. Gopal ◽  
P. C. Gupta ◽  
V. P. Aggarwala ◽  
S. P. Garg

Phthaleins (PE) with a chiral carbon atom - phenyl phenol PE, phenyl resorcinol PE, phenyl catechol PE, phenyl quinol PE, phenyl pyrogallol PE, phenyl phloroglucinol PE and phenyl orcinol PE have been obtained by condensing 2-benzoyl benzoic acid with appropriate phenols. The structure of phenyl resorcinol phthalein, which was found to exist in two isomeric forms, based on chemical reactions and spectral data has been discussed. The Amax values for most of the dyes were found higher than their analogous phthaleins.


1975 ◽  
Vol 30 (3-4) ◽  
pp. 169-174 ◽  
Author(s):  
W. Gombler ◽  
F. Seel

The reaction of trifluoromethylchlorosulfane with an excess of hydrogensulfide yields trifluoromethyldisulfane. The new compound has been characterised by its IR, Raman, 19F and 1H NMR, UV and mass spectrum, melting and boiling point and by vapour pressure data. The result of some chemical reactions are reported. Furthermore, previously unreported NMR and mass spectral data of CF3SH, CF3S3CF3 and CF3S4CF3 are given.


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