Influence of gel-formation conditions on phase changes in polymer aluminosilicate gels of mullite composition

Refractories ◽  
1991 ◽  
Vol 32 (1-2) ◽  
pp. 14-19
Author(s):  
A. V. Galakhov ◽  
V. Ya. Shevchenko
Keyword(s):  
Phase Changes ◽  
Gel Formation ◽  
Formation Conditions ◽  
Mullite Composition

Role and properties of the gel formed during nuclear glass alteration: importance of gel formation conditions

2001 ◽  
Vol 298 (1-2) ◽  
pp. 1-10 ◽  
Author(s):  
S. Gin ◽  
I. Ribet ◽  
M. Couillard
Keyword(s):  
Gel Formation ◽  
Formation Conditions

Change in molecular weight retention curves of ultrafiltration membranes with respect to lignosulfonates under gel formation conditions

2002 ◽  
Vol 210 (2) ◽  
pp. 183-196 ◽  
Author(s):  
Eugene Tsapiuk ◽  
Victor Kochkonan ◽  
Vasil Badekha
Keyword(s):  
Molecular Weight ◽  
Gel Formation ◽  
Weight Retention ◽  
Ultrafiltration Membranes ◽  
Formation Conditions

The Interpretation of Crystal Lattice Images

1972 ◽  
Vol 30 ◽  
pp. 550-551
Author(s):  
J. M. Cowley ◽  
Sumio Iijima
Keyword(s):  
Crystal Orientation ◽  
Diffraction Theory ◽  
Phase Changes ◽  
Electron Wave ◽  
Crystal Lattices ◽  
Heavy Atoms ◽  
Lattice Images ◽  
The Right ◽  
Intuitive Interpretation ◽  
Suitable Approximation

The imaging of detailed structures of crystal lattices with 3 to 4Å resolution, given the correct conditions of microscope defocus and crystal orientation and thickness, has been used by Iijima (this conference) for the study of new types of crystal structures and the defects in known structures associated with fluctuations of stoichiometry. The image intensities may be computed using n-beam dynamical diffraction theory involving several hundred beams (Fejes, this conference). However it is still important to have a suitable approximation to provide an immediate rough estimate of contrast and an evaluation of the intuitive interpretation in terms of an amplitude object.For crystals 100 to 150Å thick containing moderately heavy atoms the phase changes of the electron wave vary by about 10 radians suggesting that the “optimum defocus” theory of amplitude contrast for thin phase objects due to Scherzer and others can not apply, although it does predict the right defocus for optimum imaging.

Remote diagnostics of vibrations of dynamic objects by Doppler microwave sensors

Metrologiya ◽  
2020 ◽  
pp. 25-42
Author(s):  
Dmitrii V. Khablov
Keyword(s):  
Intelligent Systems ◽  
Electromagnetic Waves ◽  
Continuous Monitoring ◽  
Phase Changes ◽  
Vibration Diagnostics ◽  
Remote Diagnostics ◽  
Active Vibration ◽  
Dynamic Objects ◽  
Microwave Sensors ◽  
Non Destructive

This paper describes a promising method for non-contact vibration diagnostics based on the use of Doppler microwave sensors. In this case, active irradiation of the object with electromagnetic waves and the allocation of phase changes using two-channel quadrature processing of the received reflected signal are used. The modes of further fine analysis of the resulting signal using spectral or wavelet transformations depending on the nature of the active vibration are considered. The advantages of this non-contact and remote vibration analysis method for the study of complex dynamic objects are described. The convenience of the method for machine learning and use in intelligent systems of non-destructive continuous monitoring of the state of these objects by vibration is noted.

A UNIQUE FINDING OF ZIRCON INTO BADDELEYITE TRANSFORMATION (THE ICHETJU ORE OCCURRENCE, THE MIDDLE TIMAN)

2018 ◽  
pp. 27-35
Author(s):  
S. G. Skublov ◽  
A. O. Krasotkina ◽  
A. B. Makeyev ◽  
O. L. Galankina ◽  
A. E. Melnik
Keyword(s):  
High Temperature ◽  
Experimental Studies ◽  
Middle Timan ◽  
Natural Analogues ◽  
Opposite Situation ◽  
Formation Conditions

Findings of the growth relationships between baddeleyite and zircon are rare, due to significant differences in the formation conditions of the minerals. A reaction replacement (partial to complete) of baddeleyite by zircon is possible during metamorphism accompanied by the interaction with high-Si fluids. The opposite situation, when zircon is replaced by baddeleyite, is extremely rare in the nature. Transformation of zircon from polymineral (compound) ore occurrence Ichetju (the Middle Timan) with the formation of microaggregates of baddeleyite, ratile and florencite has been found out. The size of the largest segregations of baddeleyite does not exceed 10 microns in diameter. Microaggregates are unevenly related to the rim of zircon with a thickness of 10 to 50 rfn, voids and cracks across the grain. Altered zircon rim (a mixture of newly formed minerals) is characterized by sharply increased composition of REE (especially LREE), Y, Nb, Ca, Ti. The composition of Th and U also increases. An overview of the experimental studies on the reaction between zircon and baddeleyite and single natural analogues allows to make a conclusion that the most likely mechanism of the transformation of zircon from ore occurrence Ichetju to baddeleyite (intergrowth with ratile and florencite) is due to the effect of interaction of primary zircon with high-temperature (higher than 500—600°C) alkaline fluids transporting HFSE (REE, Y, Nb, Ti). This is indirectly confirmed by the findings of zircon with anomalous high composition of Y and REE up to 100000 and 70000 ppm respectively.

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