Development and application of metal organic framework/chitosan foams based on ultrasound-assisted solid-phase extraction coupling to UPLC-MS/MS for the determination of five parabens in water

2018 ◽  
Vol 410 (25) ◽  
pp. 6619-6632 ◽  
Author(s):  
Shuo Li ◽  
Mengtian Jia ◽  
Hongqiao Guo ◽  
Xiaohong Hou
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Metal Organic Framework ◽  
Phase Extraction ◽  
Metal Organic ◽  
Ultrasound Assisted ◽  
Organic Framework

Ultrasound-assisted dispersive magnetic solid phase extraction based on metal–organic framework/1-(2-pyridylazo)-2-naphthol modified magnetite nanoparticle composites for speciation analysis of inorganic tin

2019 ◽  
Vol 43 (12) ◽  
pp. 4929-4936 ◽  
Author(s):  
Majid Esmaeilzadeh
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Metal Organic Framework ◽  
Magnetic Solid Phase Extraction ◽  
Speciation Analysis ◽  
Phase Extraction ◽  
Metal Organic ◽  
Magnetic Solid ◽  
Ultrasound Assisted ◽  
Organic Framework

A novel magnetic metal–organic framework (MMOF) consisting of MIL-101(Cr) and 1-(2-pyridylazo)-2-naphthol-modified magnetite nanoparticles was synthesized and utilized for the ultrasound-assisted magnetic solid phase extraction and speciation analysis of Sn(ii) and Sn(iv) at trace amounts.

scholarly journals Chromium-based metal organic framework for pipette tip micro-solid phase extraction: an effective approach for determination of methyl and propyl parabens in wastewater and shampoo samples

BMC Chemistry ◽  
2021 ◽  
Vol 15 (1) ◽  
Author(s):  
Massoud Kaykhaii ◽  
Sayyed Hossein Hashemi ◽  
Fariba Andarz ◽  
Amin Piri ◽  
Ghasem Sargazi ◽  
...  
Keyword(s):  
Detection Limit ◽  
Solid Phase Extraction ◽  
Solid Phase ◽  
Metal Organic Framework ◽  
Phase Extraction ◽  
Propyl Paraben ◽  
Metal Organic ◽  
Pipette Tip ◽  
Organic Framework

Abstract Background A chromium-based metal organic framework was synthesized and employed as an efficient sorbent for pipette tip micro-solid phase extraction and preconcentration of parabens from wastewater and shampoo samples up to sub-ppb level before their spectrophotometric analysis. Results Factors affecting preconcentration including volume and type of solvent, amount of sorbent, number of extraction, and volume and pH of samples were optimized employing one-variable-at-a-time and response surface methodology. Obtained analytical characteristics of the method proves its usefulness for analysis of real samples. Linear range of the method for parabens was 1.0–200.0 μg/L. Detection limit of the protocol was 0.24 µg/L for propyl paraben and 0.25 µg/L for methyl paraben. Reproducibility of the protocol defined as % RSD was better than 5.78%. Synthesized adsorbent can be re-used for at least 20 extractions. Conclusion The method showed a good detection limit and precision for determination of methyl- and propyl-paraben in wastewater and shampoo samples.

Application of a Zn(ii) based metal–organic framework as an efficient solid-phase extraction sorbent for preconcentration of plasticizer compounds

RSC Advances ◽  
2016 ◽  
Vol 6 (46) ◽  
pp. 40211-40218 ◽  
Author(s):  
Elham Tahmasebi ◽  
Mohammad Yaser Masoomi ◽  
Yadollah Yamini ◽  
Ali Morsali
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Low Cost ◽  
Metal Organic Framework ◽  
Phase Extraction ◽  
Metal Organic ◽  
Organic Framework

A solid-phase extraction (SPE) sorbent, a Zn(ii) based metal–organic framework, was prepared via a simple, solventless, green and a low-cost mechanosynthesis process.

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