Theoretical and experimental study on the size- and morphology-dependent electrochemical thermodynamics of nano-silver electrode

2020 ◽  
Vol 24 (3) ◽  
pp. 557-569 ◽  
Author(s):  
Qingshan Fu ◽  
Hongxu Gao ◽  
Wengang Qu ◽  
Fengqi Zhao ◽  
Yongqiang Xue ◽  
...  
2020 ◽  
Vol 12 (2) ◽  
pp. 125-131
Author(s):  
Jixing Yang

This paper studies the application of nano drug carrier in the detection of human hemoglobin content. Taking nano modified electrode as nano drug carrier, the application of nano silver particle modified silver electrode and nano poly thionine modified electrode in the detection of human hemoglobin content is studied. Atomic force microscope, UV-Vis and FT-IR are used to characterize the nano poly(thionine), and the electrochemical properties of nano poly(thionine) modified electrode. The silver electrode decorated with nano silver particles is made. The electrochemical behavior of hemoglobin on the modified electrode is studied. The experimental results show that a pair of redox peaks appear in the silver electrode modified by nano silver particles. With the increase of Hb concentration, the redox peak current in the cyclic voltammogram of the silver electrode modified by nano silver particles increases correspondingly, and the hemoglobin has a good current response on the silver electrode modified by nano silver particles, which is a kind of adsorption current. The electrochemical activity of nano poly thionine shows a decreasing tendency with pH value. After adding hemoglobin, there is a significant reduction peak near –0.4 V. With the increase of hemoglobin concentration, the reduction peak current increases accordingly. The nano poly thionine modified electrode has a catalytic effect on the reduction of hemoglobin. The results show that the two nano drug carriers, nano poly thionine modified electrode and nano silver particle modified silver electrode, can effectively analyze and determine human hemoglobin.


2020 ◽  
Vol 146 ◽  
pp. 109617
Author(s):  
Qingshan Fu ◽  
Wengang Qu ◽  
Hongxu Gao ◽  
Libai Xiao ◽  
Shiyao Niu ◽  
...  

2021 ◽  
Vol 25 (9) ◽  
pp. 107-112
Author(s):  
P. Maheswari ◽  
S.G. Gunasekaran ◽  
Stephen L. Devaraj

In this present work, we have investigated the arsenic, fluoride and nitrate removal by the poly (ether-ether-sulfone) (PEES)/nano-silver hybrid membranes effectively prepared by the non solvent induced phase separation. The prepared membranes were characterized by thermal and mechanical properties to investigate the influence of nano-silver on the final properties of the membranes. Hence, our experimental study is based on arsenic (III) and arsenic (V) rejection studies attempted at different pH. The results of this study revealed the As (V) removal by NF with a high rejection of 99.98% compared to As (III). Fluoride and nitrate studies were carried out at neutral pH and it showed more than 80% rejection. Based on this investigation, it was concluded that the PEES/nano-silver membranes were effectively applicable to remove hazardous metal ions.


2011 ◽  
Vol 694 ◽  
pp. 284-287 ◽  
Author(s):  
Wei Wei Li ◽  
Lu Hai Li ◽  
Xu Wei Hu ◽  
Hua Fang ◽  
Xian Leng ◽  
...  

In order to compare different concentration modes' influence on the nano-silver particle size and morphology,we use three methods to refine nano-silver solution prepared in the lab as:1 centrifugal the solution directly,2 deposit the solution with acetone,3 centrifugal the solution with acetone added.Then test the solution processed with particle size distribution,UV-vis and SEM.The result shows that:the particle sizes of the nano-silver solutions enriched with the three methods are 162.5nm,163.5nm,164nm;the peak of the UV-vis absorption curve are 425nm, 426.5nm,427nm,we can see that different methods of enrichment have less influence on the nano-silver particles' size and morphology. Also the same conclusion can be drawn from SEM test.


Author(s):  
Norio Baba ◽  
Norihiko Ichise ◽  
Syunya Watanabe

The tilted beam illumination method is used to improve the resolution comparing with the axial illumination mode. Using this advantage, a restoration method of several tilted beam images covering the full azimuthal range was proposed by Saxton, and experimentally examined. To make this technique more reliable it seems that some practical problems still remain. In this report the restoration was attempted and the problems were considered. In our study, four problems were pointed out for the experiment of the restoration. (1) Accurate beam tilt adjustment to fit the incident beam to the coma-free axis for the symmetrical beam tilting over the full azimuthal range. (2) Accurate measurements of the optical parameters which are necessary to design the restoration filter. Even if the spherical aberration coefficient Cs is known with accuracy and the axial astigmatism is sufficiently compensated, at least the defocus value must be measured. (3) Accurate alignment of the tilt-azimuth series images.


1962 ◽  
Vol 5 (4) ◽  
pp. 387-394 ◽  
Author(s):  
Bruce Quarrington ◽  
Jerome Conway ◽  
Nathan Siegel
Keyword(s):  

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