Synthesis and Characterization of a Novel Preceramic Polymer for SiBNC-Ti Ceramics

Author(s):  
Yong Liu ◽  
Zicheng Tang ◽  
Shaofei Wang ◽  
Rogers Tusiime ◽  
Jian Shen ◽  
...  
Author(s):  
Maria J.S. Parvulescu ◽  
Kara L. Martin ◽  
Pavel Mogilevsky ◽  
Tulsi A. Patel ◽  
Dayton P. Street ◽  
...  

2010 ◽  
Vol 45 (4) ◽  
pp. 1025-1031 ◽  
Author(s):  
Yoon Joo Lee ◽  
Jung Hyun Lee ◽  
Soo Ryong Kim ◽  
Woo Teck Kwon ◽  
Hyunju Oh ◽  
...  

RSC Advances ◽  
2015 ◽  
Vol 5 (105) ◽  
pp. 86214-86218 ◽  
Author(s):  
Xiaojuan Zhang ◽  
Jing Li ◽  
Ke Cao ◽  
Yong Yi ◽  
Junxiao Yang ◽  
...  

A new poly(norbornenyldecaborane-co-hexadiene) (P(NB-co-DE)) copolymer as a kind of boron carbide preceramic polymer was synthesized by the ROMP reaction. And it was used to fabricate B–C polymer hollow microspheres by microencapsulation.


2018 ◽  
Vol 19 (5) ◽  
pp. 956-964 ◽  
Author(s):  
Chenyu Zhang ◽  
Yong Liu ◽  
Yongjie Cui ◽  
Minqiang Jiang ◽  
Keqing Han ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-4
Author(s):  
Feng Gao ◽  
Zhijian Peng ◽  
Xiuli Fu

Silica nanospheres have attracted tremendous interest due to their importance in extensive applications. However, the direct large-scale fabrication of silica nanospheres with controlled morphology and high purity remains a significant challenge. In this work, silica nano-/submicron spheres were successfully synthesized by a simple method through pyrolysis of an amorphous polysilazane preceramic powder with catalyst FeCl2. The synthesized spheres possess well-designed shape with diameter of 600–800 nm and high purity. The surfaces of the spheres are smooth and clean without any flaws. Besides, the spheres are identified as amorphous silica, and their growth mechanism was also proposed.


1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.


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