Spray pyrolysis synthesis of mesoporous TiO2 microspheres and their post modification for improved photocatalytic activity

2018 ◽  
Vol 35 (12) ◽  
pp. 2480-2486 ◽  
Author(s):  
Jaehyung Choi ◽  
Kye Sang Yoo ◽  
Jinsoo Kim
2009 ◽  
Vol 1 (1) ◽  
pp. 12-16 ◽  
Author(s):  
Jing Mao-Xiang ◽  
Jiang Xue-Qin ◽  
Li Wang-Xing ◽  
Li Dong-Hong ◽  
Wang Zhou

2012 ◽  
Vol 578 ◽  
pp. 99-104
Author(s):  
Yang Lin Liu ◽  
Xue Chen Duan ◽  
Shu Yun Liu ◽  
Yan Yan Liu

Mesoporous TiO2 microspheres were prepared by Ultrasonic-Hydrothermal Process with tetrabutyltitanate as titanium resource and octadecylamine as template. The effects of temperature and time of hytrothermol process, and calcination temperature on the structure had been investigated via XRD,SEM,TEM.The results indicated it will be better hythrothermol treating 20h at 120°Cand then heat-treating 4h at 400°C. A high surface area of 261.7 m2/g and pore volume of 0.28cm3/g was obtained in the corresponding sample with quite narrow distribution,and centering at 4.3nm in diameter.TiO2 frame was highly crystallized, showed the characteristic of pure anataste, with average crystal size of 10.0nm. The as-prepared sample possess a morphology of microspheres with diameter about 100-300nm.The photocatalytic activity was valuated by photodegradation of methly orange. The resultes indicated 99.79% of methly orange in the solution was removed after 30min photocatalytic treatment.


Author(s):  
Andre L. da Silva ◽  
Fabiane J. Trindade ◽  
Jean-Lou Dalmasso ◽  
Bruno Ramos ◽  
Antonio Carlos S.C. Teixeira ◽  
...  

Author(s):  
Roberta Silva Pugina ◽  
Eloísa Garibalde Hilário ◽  
Euzane Gomes da Rocha ◽  
Manoel L. da Silva-Neto ◽  
Avishek Das ◽  
...  

RSC Advances ◽  
2017 ◽  
Vol 7 (13) ◽  
pp. 8004-8010 ◽  
Author(s):  
Qi Liu ◽  
Beibei Zhou ◽  
Miao Xu ◽  
Guobing Mao

Hybrid TiO2/ZIF-8 nanobeads have been prepared by decorating the surface of mesoporous TiO2 spheres with ZIF-8 nanoparticles and enhanced photocatalytic activity of Cr(vi) reduction than pristine TiO2 beads due to their hybrid nanostructures.


2010 ◽  
Vol 519 (1) ◽  
pp. 101-105 ◽  
Author(s):  
Li Jinlong ◽  
Ma Xinxin ◽  
Sun Mingren ◽  
Xiaomin Li ◽  
Song Zhenlun

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