Sample preparation techniques for determining semi-volatile organic compounds in nuclear defense materials production waste

1996 ◽  
Vol 738 (2) ◽  
pp. 215-224
Author(s):  
J. Ward Hills
2007 ◽  
Vol 1153 (1-2) ◽  
pp. 130-144 ◽  
Author(s):  
Kristof Demeestere ◽  
Jo Dewulf ◽  
Bavo De Witte ◽  
Herman Van Langenhove

Author(s):  
Andrei V. Oberenko ◽  
Sergey V. Kachin ◽  
Sergey A. Sagalakov

A device and a method for sample preparation have been developed, which make it possible to implement successive stages of thermal separation of volatile components from a solid (liquid) matrix, their capture from the gas phase by a solid sorbent, and liquid microextraction of sorbates for further gas chromatographic analysis. The device and the algorithm of its application for GC–MS determination of a number of volatile organic compounds from matrices with complex chemical composition have been tested


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