Hydrocarbon-bearing fluid inclusions in calcite-filled horizontal fractures from mature Posidonia Shale (Hils Syncline, NW Germany)

1995 ◽  
Vol 9 (5) ◽  
pp. 363-370 ◽  
Author(s):  
J. Jochum ◽  
G. Friedrich ◽  
D. Leythaeuser ◽  
R. Littke ◽  
B. Ropertz
Author(s):  
Walter Riegel ◽  
Hartmut Loh ◽  
Bernd Maul ◽  
Michael Prauss

Author(s):  
George Guthrie ◽  
David Veblen

The nature of a geologic fluid can often be inferred from fluid-filled cavities (generally <100 μm in size) that are trapped during the growth of a mineral. A variety of techniques enables the fluids and daughter crystals (any solid precipitated from the trapped fluid) to be identified from cavities greater than a few micrometers. Many minerals, however, contain fluid inclusions smaller than a micrometer. Though inclusions this small are difficult or impossible to study by conventional techniques, they are ideally suited for study by analytical/ transmission electron microscopy (A/TEM) and electron diffraction. We have used this technique to study fluid inclusions and daughter crystals in diamond and feldspar.Inclusion-rich samples of diamond and feldspar were ion-thinned to electron transparency and examined with a Philips 420T electron microscope (120 keV) equipped with an EDAX beryllium-windowed energy dispersive spectrometer. Thin edges of the sample were perforated in areas that appeared in light microscopy to be populated densely with inclusions. In a few cases, the perforations were bound polygonal sides to which crystals (structurally and compositionally different from the host mineral) were attached (Figure 1).


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